N-acetyl-2'-O-benzyl-5'-O-[bis(4-methoxyphenyl)(phenyl)methyl]-3'-O-[(2-cyanoethoxy)(dipropan-2-ylamino)phosphanyl]-N-(2-methylpropanoyl)-cytidine

Base Information

Chemical Name:N-acetyl-2'-O-benzyl-5'-O-[bis(4-methoxyphenyl)(phenyl)methyl]-3'-O-[(2-cyanoethoxy)(dipropan-2-ylamino)phosphanyl]-N-(2-methylpropanoyl)-cytidine
CAS No.:1314972-07-0
Molecular Formula:C₄₈H₅₆N₅O₉P
Molecular Weight:877.975
Hs Code.:

N-acetyl-2'-O-benzyl-5'-O-[bis(4-methoxyphenyl)(phenyl)methyl]-3'-O-[(2-cyanoethoxy)(dipropan-2-ylamino)phosphanyl]-N-(2-methylpropanoyl)-cytidine

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Chemical Property of N-acetyl-2'-O-benzyl-5'-O-[bis(4-methoxyphenyl)(phenyl)methyl]-3'-O-[(2-cyanoethoxy)(dipropan-2-ylamino)phosphanyl]-N-(2-methylpropanoyl)-cytidine

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Technology Process of N-acetyl-2'-O-benzyl-5'-O-[bis(4-methoxyphenyl)(phenyl)methyl]-3'-O-[(2-cyanoethoxy)(dipropan-2-ylamino)phosphanyl]-N-(2-methylpropanoyl)-cytidine

There total 2 articles about N-acetyl-2'-O-benzyl-5'-O-[bis(4-methoxyphenyl)(phenyl)methyl]-3'-O-[(2-cyanoethoxy)(dipropan-2-ylamino)phosphanyl]-N-(2-methylpropanoyl)-cytidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₉H₃₉N₃O₈

: 132133-40-5
chloro-(2-cyanoethyl)-diisopropylaminophosphane

: 1314972-07-0
N-acetyl-2'-O-benzyl-5'-O-[bis(4-methoxyphenyl)(phenyl)methyl]-3'-O-[(2-cyanoethoxy)(dipropan-2-ylamino)phosphanyl]-N-(2-methylpropanoyl)-cytidine

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ja2068774

Reference yield:

: C₁₈H₂₁N₃O₆

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 1314972-07-0
N-acetyl-2'-O-benzyl-5'-O-[bis(4-methoxyphenyl)(phenyl)methyl]-3'-O-[(2-cyanoethoxy)(dipropan-2-ylamino)phosphanyl]-N-(2-methylpropanoyl)-cytidine

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 2 h / 20 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

With pyridine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran;
DOI:10.1021/ja2068774