2-bromo-5,6-dimethyl-1H-benzo[d]imidazole

Base Information

Chemical Name:2-bromo-5,6-dimethyl-1H-benzo[d]imidazole
CAS No.:1189164-12-2
Molecular Formula:C₉H₉BrN₂
Molecular Weight:225.088
Hs Code.:
DSSTox Substance ID:DTXSID10704663
Wikidata:Q82637144
Mol file:1189164-12-2.mol

Synonyms:2-bromo-5,6-dimethyl-1H-benzo[d]imidazole;1189164-12-2;2-Bromo-5,6-dimethyl-1H-benzimidazole;SCHEMBL1006779;DTXSID10704663;FT-0767268;F31324

Suppliers and Price of 2-bromo-5,6-dimethyl-1H-benzo[d]imidazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
2-Bromo-5,6-dimethyl-1H-benzo[d]imidazole 95%
5g
$ 962.00

Matrix Scientific
2-Bromo-5,6-dimethyl-1H-benzo[d]imidazole 95%
25g
$ 2886.00

Crysdot
2-Bromo-5,6-dimethyl-1H-benzo[d]imidazole 97%
25g
$ 2352.00

Crysdot
2-Bromo-5,6-dimethyl-1H-benzo[d]imidazole 97%
5g
$ 937.00

Crysdot
2-Bromo-5,6-dimethyl-1H-benzo[d]imidazole 97%
1g
$ 419.00

Crysdot
2-Bromo-5,6-dimethyl-1H-benzo[d]imidazole 97%
10g
$ 1409.00

Alichem
2-Bromo-5,6-dimethyl-1H-benzo[d]imidazole
25g
$ 3283.00

Alichem
2-Bromo-5,6-dimethyl-1H-benzo[d]imidazole
10g
$ 2170.80

Alichem
2-Bromo-5,6-dimethyl-1H-benzo[d]imidazole
5g
$ 1433.80

Total 2 raw suppliers

Chemical Property of 2-bromo-5,6-dimethyl-1H-benzo[d]imidazole

Chemical Property:

XLogP3:3.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:223.99491
Heavy Atom Count:12
Complexity:174

Purity/Quality:

97% ^*data from raw suppliers

2-Bromo-5,6-dimethyl-1H-benzo[d]imidazole 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC2=C(C=C1C)N=C(N2)Br

Technology Process of 2-bromo-5,6-dimethyl-1H-benzo[d]imidazole

There total 3 articles about 2-bromo-5,6-dimethyl-1H-benzo[d]imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 3287-79-4
5,6-dimethyl-2-mercaptobenzimidazole

: 1189164-12-2
2-bromo-5,6-dimethyl-1H-benzo[d]imidazole

Guidance literature:: With hydrogen bromide; bromine; acetic acid; In water; at 23 ℃; for 4.5h;
DOI:10.1021/jm1000248

Reference yield: 32.0%

: 3287-79-4
5,6-dimethyl-1,3-dihydro-2H-benzoimidazole-2-thione

: 1189164-12-2
2-bromo-5,6-dimethyl-1H-benzo[d]imidazole

Guidance literature:: 5,6-dimethyl-1,3-dihydro-2H-benzoimidazole-2-thione; With hydrogen bromide; bromine; acetic acid; In water; at 20 ℃; for 4.66667h; Cooling;

With sodium hydroxide; In water; at 0 ℃; pH=4;
DOI:10.1016/j.bmc.2010.01.039

Reference yield:

: 3171-45-7
4,5-dimethyl-1,2-phenylenediamine

: 1189164-12-2
2-bromo-5,6-dimethyl-1H-benzo[d]imidazole

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol; water / 3 h / Reflux

2: hydrogen bromide; bromine; acetic acid / water / 4.5 h / 0 - 23 °C

With hydrogen bromide; bromine; acetic acid; In ethanol; water;
DOI:10.3762/bjoc.9.103