4-2-[2-(2-methoxyethoxy)ethoxy]ethoxycyclohexanone

Base Information

• Chemical Name: 4-2-[2-(2-methoxyethoxy)ethoxy]ethoxycyclohexanone
• CAS No.: 1315073-06-3
• Molecular Formula: C₁₃H₂₄O₅
• Molecular Weight: 260.331
• Mol file: 1315073-06-3.mol

Synonyms:

Chemical Property of 4-2-[2-(2-methoxyethoxy)ethoxy]ethoxycyclohexanone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-2-[2-(2-methoxyethoxy)ethoxy]ethoxycyclohexanone

There total 4 articles about 4-2-[2-(2-methoxyethoxy)ethoxy]ethoxycyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.4%

1,4-Cyclohexanediol (556-48-9) + toluene-4-sulfonic acid 2-(2-methoxyethoxy)ethyl ester (50586-80-6,58320-73-3) → 4-2-[2-(2-methoxyethoxy)ethoxy]ethoxycyclohexanone (1315073-06-3)

Guidance literature:

1,4-Cyclohexanediol; With sodium hydride; In N,N-dimethyl-formamide; at 20 - 50 ℃; for 6h; Inert atmosphere;

toluene-4-sulfonic acid 2-(2-methoxyethoxy)ethyl ester; In N,N-dimethyl-formamide; at 20 ℃; for 2h; Inert atmosphere;

With potassium dichromate; sulfuric acid; In water;

DOI:10.1039/c1jm11288k

Reference yield:

4-ethoxycyclohexan-1-ol (106349-63-7) → 4-2-[2-(2-methoxyethoxy)ethoxy]ethoxycyclohexanone (1315073-06-3)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium dichromate; sulfuric acid

2: potassium dichromate; sulfuric acid

With potassium dichromate; sulfuric acid;

DOI:10.1039/c7tb01291h

Reference yield:

4-ethoxycyclohexan-1-one (23510-92-1) → 4-2-[2-(2-methoxyethoxy)ethoxy]ethoxycyclohexanone (1315073-06-3)

Guidance literature:

With potassium dichromate; sulfuric acid;

DOI:10.1039/c7tb01291h

upstream raw materials:

1,4-Cyclohexanediol

toluene-4-sulfonic acid 2-(2-methoxyethoxy)ethyl ester

4-ethoxycyclohexan-1-ol

4-ethoxycyclohexan-1-one