2-(1-Benzyl-2-{(2R,3S,4R,5R)-5-(6-dimethylamino-purin-9-yl)-4-hydroxy-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-3-yloxy}-ethyl)-isoindole-1,3-dione

Base Information

Chemical Name:2-(1-Benzyl-2-{(2R,3S,4R,5R)-5-(6-dimethylamino-purin-9-yl)-4-hydroxy-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-3-yloxy}-ethyl)-isoindole-1,3-dione
CAS No.:74397-40-3
Molecular Formula:C₄₉H₄₆N₆O₇
Molecular Weight:830.94
Hs Code.:

2-(1-Benzyl-2-{(2R,3S,4R,5R)-5-(6-dimethylamino-purin-9-yl)-4-hydroxy-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-3-yloxy}-ethyl)-isoindole-1,3-dione

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Chemical Property of 2-(1-Benzyl-2-{(2R,3S,4R,5R)-5-(6-dimethylamino-purin-9-yl)-4-hydroxy-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-3-yloxy}-ethyl)-isoindole-1,3-dione

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Technology Process of 2-(1-Benzyl-2-{(2R,3S,4R,5R)-5-(6-dimethylamino-purin-9-yl)-4-hydroxy-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-3-yloxy}-ethyl)-isoindole-1,3-dione

There total 1 articles about 2-(1-Benzyl-2-{(2R,3S,4R,5R)-5-(6-dimethylamino-purin-9-yl)-4-hydroxy-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-3-yloxy}-ethyl)-isoindole-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 57881-34-2
5'-O-monomethoxytrityl-N₆,N₆-dimethyladenosine

: 70451-00-2
Trifluoro-methanesulfonic acid (R)-2-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-3-phenyl-propyl ester

: 74397-40-3
2-(1-Benzyl-2-{(2R,3S,4R,5R)-5-(6-dimethylamino-purin-9-yl)-4-hydroxy-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-3-yloxy}-ethyl)-isoindole-1,3-dione

: 74397-43-6
2-(1-Benzyl-2-{(2R,3R,4R,5R)-2-(6-dimethylamino-purin-9-yl)-4-hydroxy-5-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-3-yloxy}-ethyl)-isoindole-1,3-dione

Guidance literature:: sodium hydride; In 1,4-dioxane; for 72h; Title compound not separated from byproducts; Ambient temperature;
DOI:10.1021/jo01308a012

Reference yield:

: 74397-40-3
2-(1-Benzyl-2-{(2R,3S,4R,5R)-5-(6-dimethylamino-purin-9-yl)-4-hydroxy-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-3-yloxy}-ethyl)-isoindole-1,3-dione

: 74397-43-6
2-(1-Benzyl-2-{(2R,3R,4R,5R)-2-(6-dimethylamino-purin-9-yl)-4-hydroxy-5-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-3-yloxy}-ethyl)-isoindole-1,3-dione

: 74397-45-8
2-{1-[(2R,3S,4R,5R)-5-(6-Dimethylamino-purin-9-yl)-4-hydroxy-2-hydroxymethyl-tetrahydro-furan-3-yloxymethyl]-2-phenyl-ethyl}-isoindole-1,3-dione

: 74397-46-9
2-{1-Benzyl-2-[(2R,3R,4R,5R)-2-(6-dimethylamino-purin-9-yl)-4-hydroxy-5-hydroxymethyl-tetrahydro-furan-3-yloxy]-ethyl}-isoindole-1,3-dione

Guidance literature:: With acetic acid; for 24h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature;
DOI:10.1021/jo01308a012