O-α-D-Glucopyranosyl-(1->6)-O-β-D-glucopyranosyl-(1->6)-N--α-D-glucopyranosylamine

Base Information

Chemical Name:O-α-D-Glucopyranosyl-(1->6)-O-β-D-glucopyranosyl-(1->6)-N--α-D-glucopyranosylamine
CAS No.:131176-21-1
Molecular Formula:C₂₇H₄₅N₃O₁₉
Molecular Weight:715.663
Hs Code.:

O-α-D-Glucopyranosyl-(1->6)-O-β-D-glucopyranosyl-(1->6)-N-<L-aspart-1-oyl-(L-proline)-4-oyl>-α-D-glucopyranosylamine

Synonyms:

Suppliers and Price of O-α-D-Glucopyranosyl-(1->6)-O-β-D-glucopyranosyl-(1->6)-N--α-D-glucopyranosylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O-α-D-Glucopyranosyl-(1->6)-O-β-D-glucopyranosyl-(1->6)-N--α-D-glucopyranosylamine

Chemical Property:

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Technology Process of O-α-D-Glucopyranosyl-(1->6)-O-β-D-glucopyranosyl-(1->6)-N--α-D-glucopyranosylamine

There total 21 articles about O-α-D-Glucopyranosyl-(1->6)-O-β-D-glucopyranosyl-(1->6)-N--α-D-glucopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 131110-17-3,131176-94-8,138921-64-9,138921-66-1
O-α-D-glucopyranosyl-(1->6)-O-β-D-glucopyranosyl-(1->6)-2,3-di-O-benzyl-1-N--α-D-glucopyranosylamine

: 131088-79-4,131176-21-1,138921-65-0,138921-67-2
O-α-D-Glucopyranosyl-(1->6)-O-β-D-glucopyranosyl-(1->6)-N--α-D-glucopyranosylamine

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; water; for 24h;
DOI:10.1016/0008-6215(90)80006-O

Reference yield: 82.0%

: 131110-17-3,131176-94-8,138921-64-9,138921-66-1
O-α-D-glucopyranosyl-(1-6)-O-β-D-glucopyranosyl-(1-6)-2,3-di-O-benzyl-1-N--β-D-glucopyranosylamine

: 131088-79-4,131176-21-1,138921-65-0,138921-67-2
O-α-D-glucopyranosyl-(1->6)-O-β-D-glucopyranosyl-(1->6)-1-N--β-D-glucopyranosylamine

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; water; for 24h;
DOI:10.1016/0008-6215(90)80006-O

Reference yield:

: 131088-76-1
N-(tert-butoxycarbonyl)-L-aspartyl-L-proline methyl ester

: 131088-79-4,131176-21-1,138921-65-0,138921-67-2
O-α-D-Glucopyranosyl-(1->6)-O-β-D-glucopyranosyl-(1->6)-N--α-D-glucopyranosylamine

Guidance literature:: Multi-step reaction with 4 steps

1: O,O-diethylcyanophosphate, Et₃N / dimethylformamide / 1) 1 h, 0 deg C, 2) 24 h, r.t.

2: 60.4 percent / 85percent HCO₂H / 5 h / Ambient temperature

3: NaOMe

4: H₂ / 10percent Pd/C / ethanol; H₂O / 24 h

With formic acid; diethyl cyanophosphonate; hydrogen; sodium methylate; triethylamine; palladium on activated charcoal; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1248/cpb.39.2699