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4-CH3C6H4SbC12H7(NO2)

Base Information
  • Chemical Name:4-CH3C6H4SbC12H7(NO2)
  • CAS No.:854832-61-4
  • Molecular Formula:C19H14NO2Sb
  • Molecular Weight:410.076
  • Hs Code.:
4-CH<sub>3</sub>C<sub>6</sub>H<sub>4</sub>SbC<sub>12</sub>H<sub>7</sub>(NO<sub>2</sub>)

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Chemical Property of 4-CH3C6H4SbC12H7(NO2)
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Technology Process of 4-CH3C6H4SbC12H7(NO2)

There total 1 articles about 4-CH3C6H4SbC12H7(NO2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With sodium acetate; tin(ll) chloride; In water; acetone; Sb-compd. dissolved in acetone, addn. of aq. NaOAc, ppt. dried in vac. desiccator, dissolved in (AcO)2O contg. concd. H2SO4, warmed to 90°C, poured on ice, ppt. washed, dissolved in acetone contg. HCl, reduced by stannous chloride; recrystn. from ethylacetate;
Guidance literature:
With zinc dust; CaCl2; In ethanol; water; redn. in ethanol/water (5:1) with zinc dust in the presence of a small amts. of CaCl2 during 4 h of refluxing;
DOI:10.1039/JR9550001662
upstream raw materials:

{2-(4-NO2C6H4C6H4)(4-CH3C6H4)SbCl3

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