2-p-tolyl-5,6,7,8,9,10,11,12-octahydro[1,2,4]triazino[1,6-f]-phenanthridin-13-ium-4-olate

Base Information

Chemical Name:2-p-tolyl-5,6,7,8,9,10,11,12-octahydro[1,2,4]triazino[1,6-f]-phenanthridin-13-ium-4-olate
CAS No.:1384852-38-3
Molecular Formula:C₂₂H₂₃N₃O
Molecular Weight:345.444
Hs Code.:

Synonyms:

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Chemical Property of 2-p-tolyl-5,6,7,8,9,10,11,12-octahydro[1,2,4]triazino[1,6-f]-phenanthridin-13-ium-4-olate

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 2-p-tolyl-5,6,7,8,9,10,11,12-octahydro[1,2,4]triazino[1,6-f]-phenanthridin-13-ium-4-olate

There total 3 articles about 2-p-tolyl-5,6,7,8,9,10,11,12-octahydro[1,2,4]triazino[1,6-f]-phenanthridin-13-ium-4-olate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 3-(4-methylphenyl)-1,2,4-triazin-5(4H)-one

: 1384852-38-3
2-p-tolyl-5,6,7,8,9,10,11,12-octahydro[1,2,4]triazino[1,6-f]-phenanthridin-13-ium-4-olate

Guidance literature:: 1-(2-chlorobenzyl)benzimidazole; With n-butyllithium; In tetrahydrofuran; at -75 ℃; for 1h; Inert atmosphere;

N,N-dimethyl-formamide; In tetrahydrofuran; at 75 ℃; for 1h; Inert atmosphere;
DOI:10.1248/cpb.c12-00342

Reference yield:

: 39739-50-9
p-toluimidic acid methyl ester hydrochloride

: 1384852-38-3
2-p-tolyl-5,6,7,8,9,10,11,12-octahydro[1,2,4]triazino[1,6-f]-phenanthridin-13-ium-4-olate

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrazine hydrate / methanol / 16 h

1.2: 5 - 10 °C

1.3: 0.5 h / Reflux

2.1: phosphorus pentoxide; toluene-4-sulfonic acid / acetonitrile / 3 h / Reflux

With phosphorus pentoxide; toluene-4-sulfonic acid; hydrazine hydrate; In methanol; acetonitrile;
DOI:10.1021/jo300697v

Reference yield:

: 104-85-8
para-methylbenzonitrile

: 1384852-38-3
2-p-tolyl-5,6,7,8,9,10,11,12-octahydro[1,2,4]triazino[1,6-f]-phenanthridin-13-ium-4-olate

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride / diethyl ether / 0 - 20 °C

2.1: hydrazine hydrate / methanol / 16 h

2.2: 5 - 10 °C

2.3: 0.5 h / Reflux

3.1: phosphorus pentoxide; toluene-4-sulfonic acid / acetonitrile / 3 h / Reflux

With hydrogenchloride; phosphorus pentoxide; toluene-4-sulfonic acid; hydrazine hydrate; In methanol; diethyl ether; acetonitrile;
DOI:10.1021/jo300697v