N-<<(2-Chloro-6-methoxy-9-acridinyl)amino>propyl>-N-<(9-acridinylamino)propyl>-N'-phenyl-N''-<6-<(4-azidobenzoyl)amino>hexyl>guanidine, 3HCl, 8H2O

Base Information

• Chemical Name: N-<<(2-Chloro-6-methoxy-9-acridinyl)amino>propyl>-N-<(9-acridinylamino)propyl>-N'-phenyl-N''-<6-<(4-azidobenzoyl)amino>hexyl>guanidine, 3HCl, 8H2O
• CAS No.: 92184-42-4
• Molecular Formula: C₅₃H₅₄ClN₁₁O₂*3ClH
• Molecular Weight: 1021.92

Synonyms:

Chemical Property of N-<<(2-Chloro-6-methoxy-9-acridinyl)amino>propyl>-N-<(9-acridinylamino)propyl>-N'-phenyl-N''-<6-<(4-azidobenzoyl)amino>hexyl>guanidine, 3HCl, 8H2O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-<<(2-Chloro-6-methoxy-9-acridinyl)amino>propyl>-N-<(9-acridinylamino)propyl>-N'-phenyl-N''-<6-<(4-azidobenzoyl)amino>hexyl>guanidine, 3HCl, 8H2O

There total 4 articles about N-<<(2-Chloro-6-methoxy-9-acridinyl)amino>propyl>-N-<(9-acridinylamino)propyl>-N'-phenyl-N''-<6-<(4-azidobenzoyl)amino>hexyl>guanidine, 3HCl, 8H2O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

N-(4-Azidobenzoyl)-N'-(phenylthiocarbamoyl)-1,6-hexanediamine (92143-62-9) + N-<<(2-Chloro-6-methoxy-9-acridinyl)amino>propyl>-N-<(9-acridinylamino)propyl>amine (92143-61-8) → N-<<(2-Chloro-6-methoxy-9-acridinyl)amino>propyl>-N-<(9-acridinylamino)propyl>-N'-phenyl-N''-<6-<(4-azidobenzoyl)amino>hexyl>guanidine, 3HCl, 8H2O (92184-42-4)

Guidance literature:

With triethylamine; mercury dichloride; In acetonitrile; for 72h; Heating;

DOI:10.1021/jo00196a004

Reference yield:

N-(4-Azidobenzoyl)-1,6-hexanediamine hydrochloride (92143-65-2) → N-<<(2-Chloro-6-methoxy-9-acridinyl)amino>propyl>-N-<(9-acridinylamino)propyl>-N'-phenyl-N''-<6-<(4-azidobenzoyl)amino>hexyl>guanidine, 3HCl, 8H2O (92184-42-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 45 percent / triethylamine / CHCl₃ / 48 h / Ambient temperature

2: 21 percent / HgCl₂, triethylamine / acetonitrile / 72 h / Heating

With triethylamine; mercury dichloride; In chloroform; acetonitrile;

DOI:10.1021/jo00196a004

Reference yield:

N-(3-Amino-propyl)-N'-(6-chloro-2-methoxy-acridin-9-yl)-propane-1,3-diamine; hydrochloride (86689-05-6) → N-<<(2-Chloro-6-methoxy-9-acridinyl)amino>propyl>-N-<(9-acridinylamino)propyl>-N'-phenyl-N''-<6-<(4-azidobenzoyl)amino>hexyl>guanidine, 3HCl, 8H2O (92184-42-4)

Guidance literature:

Multi-step reaction with 2 steps

1: various solvent(s) / 1.5 h / 100 °C

2: 21 percent / HgCl₂, triethylamine / acetonitrile / 72 h / Heating

With triethylamine; mercury dichloride; In acetonitrile;

DOI:10.1021/jo00196a004

upstream raw materials:

N-(4-Azidobenzoyl)-N'-(phenylthiocarbamoyl)-1,6-hexanediamine

N-<<(2-Chloro-6-methoxy-9-acridinyl)amino>propyl>-N-<(9-acridinylamino)propyl>amine

N-(4-Azidobenzoyl)-1,6-hexanediamine hydrochloride

N-(3-Amino-propyl)-N'-(6-chloro-2-methoxy-acridin-9-yl)-propane-1,3-diamine; hydrochloride

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