C₁₃H₁₉NO*C₂HF₃O₂

Base Information

Chemical Name:C₁₃H₁₉NO*C₂HF₃O₂
CAS No.:1447464-37-0
Molecular Formula:C₂HF₃O₂*C₁₃H₁₉NO
Molecular Weight:319.324
Hs Code.:

C<sub>13</sub>H<sub>19</sub>NO*C<sub>2</sub>HF<sub>3</sub>O<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₃H₁₉NO*C₂HF₃O₂

Chemical Property:

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Technology Process of C₁₃H₁₉NO*C₂HF₃O₂

There total 5 articles about C₁₃H₁₉NO*C₂HF₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 260352-12-3
(E)-5-(4-chlorophenyl)-2,2-diphenylpent-4-enal

: 1447464-37-0
C₁₃H₁₉NO*C₂HF₃O₂

Guidance literature:: Multi-step reaction with 4 steps

1: hydroxylamine hydrochloride; sodium methylate / methanol / 14 h / Inert atmosphere; Reflux

2: sodium cyanoborohydride; acetic acid / dichloromethane / 1.08 h / 15 - 23 °C / Inert atmosphere; Sealed tube

3: triethylamine / dichloromethane / 14 h / 23 °C / Inert atmosphere; Sealed tube

4: dichloromethane / 1 h / 23 °C / Inert atmosphere

With hydroxylamine hydrochloride; sodium methylate; sodium cyanoborohydride; acetic acid; triethylamine; In methanol; dichloromethane;
DOI:10.1021/ja402893z

Reference yield:

: 1431561-40-8
(1E, 4E)-2,2-dimethyl-5-phenylpent-4-enal oxime

: 1447464-37-0
C₁₃H₁₉NO*C₂HF₃O₂

Guidance literature:: Multi-step reaction with 3 steps

1: sodium cyanoborohydride; acetic acid / dichloromethane / 1.08 h / 15 - 23 °C / Inert atmosphere; Sealed tube

2: triethylamine / dichloromethane / 14 h / 23 °C / Inert atmosphere; Sealed tube

3: dichloromethane / 1 h / 23 °C / Inert atmosphere

With sodium cyanoborohydride; acetic acid; triethylamine; In dichloromethane;
DOI:10.1021/ja402893z

Reference yield:

: 4393-06-0
1-Phenyl-2-propen-1-ol

: 1447464-37-0
C₁₃H₁₉NO*C₂HF₃O₂

Guidance literature:: Multi-step reaction with 5 steps

1: palladium diacetate; triphenylphosphine; lithium chloride; triethyl borane; triethylamine / tetrahydrofuran; hexane / 48 h / 20 °C / Inert atmosphere

2: hydroxylamine hydrochloride; sodium methylate / methanol / 14 h / Inert atmosphere; Reflux

3: sodium cyanoborohydride; acetic acid / dichloromethane / 1.08 h / 15 - 23 °C / Inert atmosphere; Sealed tube

4: triethylamine / dichloromethane / 14 h / 23 °C / Inert atmosphere; Sealed tube

5: dichloromethane / 1 h / 23 °C / Inert atmosphere

With triethyl borane; hydroxylamine hydrochloride; sodium methylate; palladium diacetate; sodium cyanoborohydride; acetic acid; triethylamine; triphenylphosphine; lithium chloride; In tetrahydrofuran; methanol; hexane; dichloromethane; 1: |Tsuji-Trost Allylation;
DOI:10.1021/ja402893z