β-(methoxycarbonyl)-1-naphthalenebutanoic acid

Base Information

Chemical Name:β-(methoxycarbonyl)-1-naphthalenebutanoic acid
CAS No.:122872-06-4
Molecular Formula:C₁₆H₁₆O₄
Molecular Weight:272.301
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of β-(methoxycarbonyl)-1-naphthalenebutanoic acid

Chemical Property:

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Technology Process of β-(methoxycarbonyl)-1-naphthalenebutanoic acid

There total 5 articles about β-(methoxycarbonyl)-1-naphthalenebutanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 130561-76-1
3-(methoxycarbonyl)-4-(1-naphthyl)-3-butenoic acid

: 122872-06-4,119807-82-8
β-(methoxycarbonyl)-1-naphthalenebutanoic acid

: β-(methoxycarbonyl)-1,2,3,4-tetrahydro-1-naphthalene-butanoic acid

Guidance literature:: platinum(IV) oxide;

Reference yield:

: 17917-18-9
(E)-2-(1-naphthylmethylene)succinic acid 1-methyl ester

: 122872-06-4,119807-82-8
β-(methoxycarbonyl)-1-naphthalenebutanoic acid

Guidance literature:: With 5%-palladium/activated carbon; hydrogen; In methanol; under 1551.49 Torr; Autoclave;
DOI:10.1002/adsc.201800255

Reference yield:

: 66-77-3
1-naphthaldehyde

: 122872-06-4,119807-82-8
β-(methoxycarbonyl)-1-naphthalenebutanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: methanol; sodium / 12 h / Inert atmosphere; Reflux

2: 5%-palladium/activated carbon; hydrogen / methanol / 1551.49 Torr / Autoclave

With methanol; 5%-palladium/activated carbon; hydrogen; sodium; In methanol; 1: |Stobbe Condensation;
DOI:10.1002/adsc.201800255