2,5-anhydro-4-O-acetyl-3-desoxy-3-C-L-lyxose

Base Information

Chemical Name:2,5-anhydro-4-O-acetyl-3-desoxy-3-C-L-lyxose
CAS No.:79493-15-5
Molecular Formula:C₂₀H₂₀O₄S₂
Molecular Weight:388.508
Hs Code.:

2,5-anhydro-4-O-acetyl-3-desoxy-3-C-<bis(phenylthio)methyl>L-lyxose

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Chemical Property of 2,5-anhydro-4-O-acetyl-3-desoxy-3-C-L-lyxose

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Technology Process of 2,5-anhydro-4-O-acetyl-3-desoxy-3-C-L-lyxose

There total 6 articles about 2,5-anhydro-4-O-acetyl-3-desoxy-3-C-L-lyxose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79493-14-4
2,5-anhydro-4-O-acetyl-3-desoxy-3-C-L-lyxose diethylacetal

: 79493-15-5
2,5-anhydro-4-O-acetyl-3-desoxy-3-C-L-lyxose

Guidance literature:: With hydrogenchloride; In 1,2-dimethoxyethane; at 50 ℃; for 0.5h; Yield given;
DOI:10.1016/S0040-4020(01)98932-X

Reference yield:

: 70626-89-0
anion of bis(phenylthio)methane

: 79493-15-5
2,5-anhydro-4-O-acetyl-3-desoxy-3-C-L-lyxose

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / 0 °C

2: 74 percent / pyridine / 12 h / 0 °C

3: conc. HCl / 1,2-dimethoxy-ethane / 0.5 h / 50 °C

With hydrogenchloride; In tetrahydrofuran; pyridine; 1,2-dimethoxyethane;
DOI:10.1016/S0040-4020(01)98932-X

Reference yield:

: 79493-11-1
2,5-anhydro-3-C-L-lyxose diethylacetal

: 79493-15-5
2,5-anhydro-4-O-acetyl-3-desoxy-3-C-L-lyxose

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / pyridine / 12 h / 0 °C

2: conc. HCl / 1,2-dimethoxy-ethane / 0.5 h / 50 °C

With hydrogenchloride; In pyridine; 1,2-dimethoxyethane;
DOI:10.1016/S0040-4020(01)98932-X