4-(5'-(4-n-octylphenyl)-[2,2'-bithiophen]-5-yl)phenethyl methacrylate

Base Information

Chemical Name:4-(5'-(4-n-octylphenyl)-[2,2'-bithiophen]-5-yl)phenethyl methacrylate
CAS No.:1354569-30-4
Molecular Formula:C₃₄H₃₈O₂S₂
Molecular Weight:542.807
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(5'-(4-n-octylphenyl)-[2,2'-bithiophen]-5-yl)phenethyl methacrylate

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 4-(5'-(4-n-octylphenyl)-[2,2'-bithiophen]-5-yl)phenethyl methacrylate

There total 4 articles about 4-(5'-(4-n-octylphenyl)-[2,2'-bithiophen]-5-yl)phenethyl methacrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1238432-92-2
C₂₂H₂₅BrS₂

: 1312927-41-5
C₂₄H₄₀O₂Sn

: 1354569-30-4
4-(5'-(4-n-octylphenyl)-[2,2'-bithiophen]-5-yl)phenethyl methacrylate

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; at 85 ℃;
DOI:10.1002/pola.24957

Reference yield:

: 190788-89-7
C₂₂H₂₆S₂

: 1354569-30-4
4-(5'-(4-n-octylphenyl)-[2,2'-bithiophen]-5-yl)phenethyl methacrylate

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide / N,N-dimethyl-formamide / 20 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 85 °C

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; 2: Stille coupling;
DOI:10.1002/pola.24957

Reference yield:

: 1354569-22-4
C₂₆H₄₈Sn

: 1354569-30-4
4-(5'-(4-n-octylphenyl)-[2,2'-bithiophen]-5-yl)phenethyl methacrylate

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 85 °C

2: N-Bromosuccinimide / N,N-dimethyl-formamide / 20 °C

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 85 °C

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; 3: Stille coupling;
DOI:10.1002/pola.24957