Phosphoric acid (2R,3R,4R,5S,6R)-3-acetylamino-6-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4,5-dihydroxy-tetrahydro-pyran-2-yl ester (2R,3S,4R,5R,6S)-5-acetylamino-3,4,6-trihydroxy-tetrahydro-pyran-2-ylmethyl ester

Base Information

• Chemical Name: Phosphoric acid (2R,3R,4R,5S,6R)-3-acetylamino-6-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4,5-dihydroxy-tetrahydro-pyran-2-yl ester (2R,3S,4R,5R,6S)-5-acetylamino-3,4,6-trihydroxy-tetrahydro-pyran-2-ylmethyl ester
• CAS No.: 110914-57-3
• Molecular Formula: C₃₇H₄₇N₂O₁₆P
• Molecular Weight: 806.758

Synonyms:

Chemical Property of Phosphoric acid (2R,3R,4R,5S,6R)-3-acetylamino-6-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4,5-dihydroxy-tetrahydro-pyran-2-yl ester (2R,3S,4R,5R,6S)-5-acetylamino-3,4,6-trihydroxy-tetrahydro-pyran-2-ylmethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of Phosphoric acid (2R,3R,4R,5S,6R)-3-acetylamino-6-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4,5-dihydroxy-tetrahydro-pyran-2-yl ester (2R,3S,4R,5R,6S)-5-acetylamino-3,4,6-trihydroxy-tetrahydro-pyran-2-ylmethyl ester

There total 11 articles about Phosphoric acid (2R,3R,4R,5S,6R)-3-acetylamino-6-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4,5-dihydroxy-tetrahydro-pyran-2-yl ester (2R,3S,4R,5R,6S)-5-acetylamino-3,4,6-trihydroxy-tetrahydro-pyran-2-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(+)-2-acetamido-1,3,4-tri-O-acetyl-2-deoxy-α-D-glucopyranoside (10034-17-0) → Phosphoric acid (2R,3R,4R,5S,6R)-3-acetylamino-6-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4,5-dihydroxy-tetrahydro-pyran-2-yl ester (2R,3S,4R,5R,6S)-5-acetylamino-3,4,6-trihydroxy-tetrahydro-pyran-2-ylmethyl ester (110914-57-3)

Guidance literature:

Multi-step reaction with 3 steps

1: pivaloyl chloride / pyridine / 0.17 h

2: iodine / pyridine; H₂O

3: NH₃

With ammonia; iodine; pivaloyl chloride; In pyridine; water;

DOI:10.1016/S0040-4039(00)85450-7

Reference yield:

Acetic acid (2R,3S,4R,5R,6R)-4,6-diacetoxy-5-acetylamino-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-tetrahydro-pyran-3-yl ester (110914-53-9) → Phosphoric acid (2R,3R,4R,5S,6R)-3-acetylamino-6-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4,5-dihydroxy-tetrahydro-pyran-2-yl ester (2R,3S,4R,5R,6S)-5-acetylamino-3,4,6-trihydroxy-tetrahydro-pyran-2-ylmethyl ester (110914-57-3)

Guidance literature:

Multi-step reaction with 4 steps

1: H⁽¹⁺⁾

2: pivaloyl chloride / pyridine / 0.17 h

3: iodine / pyridine; H₂O

4: NH₃

With ammonia; iodine; pivaloyl chloride; hydrogen cation; In pyridine; water;

DOI:10.1016/S0040-4039(00)85450-7

Reference yield:

C43H41NO10 (110914-50-6) → Phosphoric acid (2R,3R,4R,5S,6R)-3-acetylamino-6-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4,5-dihydroxy-tetrahydro-pyran-2-yl ester (2R,3S,4R,5R,6S)-5-acetylamino-3,4,6-trihydroxy-tetrahydro-pyran-2-ylmethyl ester (110914-57-3)

Guidance literature:

Multi-step reaction with 5 steps

1: triethylamine / dioxane / 0.5 h

2: H₂O / dioxane

3: pivaloyl chloride / pyridine / 0.17 h

4: iodine / pyridine; H₂O

5: NH₃

With ammonia; water; iodine; pivaloyl chloride; triethylamine; In 1,4-dioxane; pyridine; water;

DOI:10.1016/S0040-4039(00)85450-7

upstream raw materials:

C₅₇H₆₁N₂O₂₁P

(+)-2-acetamido-1,3,4-tri-O-acetyl-2-deoxy-α-D-glucopyranoside

Acetic acid (2R,3S,4R,5R,6R)-4,6-diacetoxy-5-acetylamino-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-tetrahydro-pyran-3-yl ester

C₄₃H₄₁NO₁₀

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