Technology Process of C25H23BrCl2F2N2O4
There total 5 articles about C25H23BrCl2F2N2O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: dimethylsulfide borane complex / tetrahydrofuran / 6 h / 20 °C
2: pyridine; Dess-Martin periodane / dichloromethane; tert-butyl alcohol / 18 h
3: triethylamine; triphenylphosphine / dichloromethane / 3 h / -78 - 20 °C
4: potassium tert-butylate / tetrahydrofuran / 2 h / 20 °C
5: 3 h / 60 °C
With
pyridine; dimethylsulfide borane complex; potassium tert-butylate; Dess-Martin periodane; triethylamine; triphenylphosphine;
In
tetrahydrofuran; dichloromethane; tert-butyl alcohol;
3: Ramirez condensation;
DOI:10.1016/j.bmcl.2012.03.014
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium tert-butylate / tetrahydrofuran / 2 h / 20 °C
2: 3 h / 60 °C
With
potassium tert-butylate;
In
tetrahydrofuran;
DOI:10.1016/j.bmcl.2012.03.014
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine; triphenylphosphine / dichloromethane / 3 h / -78 - 20 °C
2: potassium tert-butylate / tetrahydrofuran / 2 h / 20 °C
3: 3 h / 60 °C
With
potassium tert-butylate; triethylamine; triphenylphosphine;
In
tetrahydrofuran; dichloromethane;
1: Ramirez condensation;
DOI:10.1016/j.bmcl.2012.03.014