Technology Process of (1,1-Dimethyl-2-phenylethyl)methylketen-N-(4-chlorphenyl)imin
There total 7 articles about (1,1-Dimethyl-2-phenylethyl)methylketen-N-(4-chlorphenyl)imin which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 6 steps
1: 71 percent / NaOEt / ethanol / 12 h / Heating
2: 70 percent / NaOH / ethane-1,2-diol / 36 h / 150 °C
3: 71 percent / N2O4 / acetic acid / 3 h / 10 °C
4: thionyl chloride / 24 h / 5 °C
5: 56 percent / Et3N / diethyl ether / 22 °C
6: 1.) PCl5, 2.) Et3N / 1.) benzene, reflux, 2.) ether, reflux
With
sodium hydroxide; thionyl chloride; phosphorus pentachloride; sodium ethanolate; dinitrogen tetraoxide; triethylamine;
In
diethyl ether; ethanol; ethylene glycol; acetic acid;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 56 percent / Et3N / diethyl ether / 22 °C
2: 1.) PCl5, 2.) Et3N / 1.) benzene, reflux, 2.) ether, reflux
With
phosphorus pentachloride; triethylamine;
In
diethyl ether;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 71 percent / N2O4 / acetic acid / 3 h / 10 °C
2: thionyl chloride / 24 h / 5 °C
3: 56 percent / Et3N / diethyl ether / 22 °C
4: 1.) PCl5, 2.) Et3N / 1.) benzene, reflux, 2.) ether, reflux
With
thionyl chloride; phosphorus pentachloride; dinitrogen tetraoxide; triethylamine;
In
diethyl ether; acetic acid;
