C₁₁H₁₃FN₂O₂S

Base Information

Chemical Name:C₁₁H₁₃FN₂O₂S
CAS No.:1356930-04-5
Molecular Formula:C₁₁H₁₃FN₂O₂S
Molecular Weight:256.301
Hs Code.:

C<sub>11</sub>H<sub>13</sub>FN<sub>2</sub>O<sub>2</sub>S

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₁H₁₃FN₂O₂S

Chemical Property:

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Technology Process of C₁₁H₁₃FN₂O₂S

There total 6 articles about C₁₁H₁₃FN₂O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3-(4-Fluoro-phenyl)-N-[2-(2-{3-(4-fluoro-phenyl)-2-[(E)-hydroxyimino]-propionylamino}-ethyldisulfanyl)-ethyl]-2-[(E)-hydroxyimino]-propionamide

: 1356930-04-5
C₁₁H₁₃FN₂O₂S

Guidance literature:: With tris-(2-carboxyethyl)-phosphine hydrochloride; In water; dimethyl sulfoxide; at 20 ℃;
DOI:10.1021/jm2016182

Reference yield:

: 7761-30-0
sodium 3-(4-fluorophenyl)-2-oxopropionate

: 1356930-04-5
C₁₁H₁₃FN₂O₂S

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / 20 °C

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / 1,4-dioxane / 20 °C

3: triethylamine / 1,4-dioxane; methanol / 20 °C

4: hydrogenchloride / 1,4-dioxane; methanol; dichloromethane / Reflux

5: tris-(2-carboxyethyl)-phosphine hydrochloride / water; dimethyl sulfoxide / 20 °C

With pyridine; hydrogenchloride; tris-(2-carboxyethyl)-phosphine hydrochloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In 1,4-dioxane; methanol; dichloromethane; water; dimethyl sulfoxide;
DOI:10.1021/jm2016182

Reference yield:

: 459-57-4
4-fluorobenzaldehyde

: 1356930-04-5
C₁₁H₁₃FN₂O₂S

Guidance literature:: Multi-step reaction with 7 steps

1: sodium acetate; acetic anhydride / Reflux

2: hydrogenchloride; water / Reflux

3: pyridine / 20 °C

4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / 1,4-dioxane / 20 °C

5: triethylamine / 1,4-dioxane; methanol / 20 °C

6: hydrogenchloride / 1,4-dioxane; methanol; dichloromethane / Reflux

7: tris-(2-carboxyethyl)-phosphine hydrochloride / water; dimethyl sulfoxide / 20 °C

With pyridine; hydrogenchloride; water; sodium acetate; tris-(2-carboxyethyl)-phosphine hydrochloride; acetic anhydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In 1,4-dioxane; methanol; dichloromethane; water; dimethyl sulfoxide;
DOI:10.1021/jm2016182