3-[4-((E)-2-Ethoxycarbonyl-vinyl)-phenyl]-2-pyridin-4-yl-4-[4-((E)-2-pyridin-4-yl-vinyl)-phenyl]-cyclobutanecarboxylic acid ethyl ester

Base Information

• Chemical Name: 3-[4-((E)-2-Ethoxycarbonyl-vinyl)-phenyl]-2-pyridin-4-yl-4-[4-((E)-2-pyridin-4-yl-vinyl)-phenyl]-cyclobutanecarboxylic acid ethyl ester
• CAS No.: 135212-23-6
• Molecular Formula: C₃₆H₃₄N₂O₄
• Molecular Weight: 558.677
• Mol file: 135212-23-6.mol

Synonyms:

Chemical Property of 3-[4-((E)-2-Ethoxycarbonyl-vinyl)-phenyl]-2-pyridin-4-yl-4-[4-((E)-2-pyridin-4-yl-vinyl)-phenyl]-cyclobutanecarboxylic acid ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-[4-((E)-2-Ethoxycarbonyl-vinyl)-phenyl]-2-pyridin-4-yl-4-[4-((E)-2-pyridin-4-yl-vinyl)-phenyl]-cyclobutanecarboxylic acid ethyl ester

There total 3 articles about 3-[4-((E)-2-Ethoxycarbonyl-vinyl)-phenyl]-2-pyridin-4-yl-4-[4-((E)-2-pyridin-4-yl-vinyl)-phenyl]-cyclobutanecarboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl 4-<2-(4-pyridyl)ethenyl>cinnamate (127943-99-1) → 3-[4-((E)-2-Ethoxycarbonyl-vinyl)-phenyl]-2-pyridin-4-yl-4-[4-((E)-2-pyridin-4-yl-vinyl)-phenyl]-cyclobutanecarboxylic acid ethyl ester (127944-00-7,135212-22-5,135212-23-6)

Guidance literature:

In solid; for 5h; Ambient temperature; Irradiation;

DOI:10.1021/ja00170a062

Reference yield:

ethyl 4-<2-(4-pyridyl)ethenyl>cinnamate (127943-99-1) → 3-[4-((E)-2-Ethoxycarbonyl-vinyl)-phenyl]-2-pyridin-4-yl-4-[4-((E)-2-pyridin-4-yl-vinyl)-phenyl]-cyclobutanecarboxylic acid ethyl ester (127944-00-7,135212-22-5,135212-23-6) + 3-[4-((E)-2-Ethoxycarbonyl-vinyl)-phenyl]-2-pyridin-4-yl-4-[4-((E)-2-pyridin-4-yl-vinyl)-phenyl]-cyclobutanecarboxylic acid ethyl ester (127944-00-7,135212-22-5,135212-23-6)

Guidance literature:

at -40 ℃; for 10h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; asymmetric synthesis in a chiral crystal;

DOI:10.1021/ja00170a062

Reference yield:

ethyl 4-<2-(4-pyridyl)ethenyl>cinnamate (127943-99-1) → 3-[4-((E)-2-Ethoxycarbonyl-vinyl)-phenyl]-2-pyridin-4-yl-4-[4-((E)-2-pyridin-4-yl-vinyl)-phenyl]-cyclobutanecarboxylic acid ethyl ester (127944-00-7,135212-22-5,135212-23-6) + 3-[4-((E)-2-Ethoxycarbonyl-vinyl)-phenyl]-2-pyridin-4-yl-4-[4-((E)-2-pyridin-4-yl-vinyl)-phenyl]-cyclobutanecarboxylic acid ethyl ester (127944-00-7,135212-22-5,135212-23-6)

Guidance literature:

at -40 ℃; for 10h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; asymmetric synthesis in a chiral crystal;

DOI:10.1021/ja00170a062

upstream raw materials:

ethyl 4-<2-(4-pyridyl)ethenyl>cinnamate