C₂₆H₂₈N₂O₄

Base Information

Chemical Name:C₂₆H₂₈N₂O₄
CAS No.:1419075-35-6
Molecular Formula:C₂₆H₂₈N₂O₄
Molecular Weight:432.519
Hs Code.:

C<sub>26</sub>H<sub>28</sub>N<sub>2</sub>O<sub>4</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₆H₂₈N₂O₄

Chemical Property:

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Technology Process of C₂₆H₂₈N₂O₄

There total 12 articles about C₂₆H₂₈N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 1419075-27-6
C₂₉H₃₆N₂O₆

: C₂₉H₃₄N₂O₅

: 1419075-34-5
C₂₆H₂₈N₂O₄

: 1419075-35-6
C₂₆H₂₈N₂O₄

Guidance literature:: With methanesulfonic acid; In dichloromethane; for 1.5h; stereoselective reaction; Inert atmosphere;
DOI:10.1002/ejoc.201200919

Reference yield:

: 1350922-84-7
(R)-benzyl [1-(2-(2-aminoethyl)-1,3-dioxan-2-yl)propan-2-yl]carbamate

: 1419075-35-6
C₂₆H₂₈N₂O₄

Guidance literature:: Multi-step reaction with 9 steps

1.1: dmap; triethylamine / dichloromethane / 0 - 20 °C

1.2: 0.5 h / 0 - 20 °C

2.1: palladium 10% on activated carbon; ammonium formate / methanol / 3 h / Reflux

3.1: magnesium sulfate / dichloromethane / Reflux

3.2: 14 h / 40 °C

4.1: palladium 10% on activated carbon; ammonium formate / methanol / 2 h / Reflux

5.1: sodium carbonate / dichloromethane; water / 3 h / 20 °C

6.1: Amberlite IRA 401 / methanol

7.1: triethylamine / toluene / 3 h / Dean-Stark; Reflux

8.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 1.5 h / -20 - 5 °C / Inert atmosphere

9.1: methanesulfonic acid / dichloromethane / 1.5 h / Inert atmosphere

With dmap; sodium tetrahydroborate; methanesulfonic acid; palladium 10% on activated carbon; ammonium formate; sodium carbonate; magnesium sulfate; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water; toluene; 3.1: |Mannich Aminomethylation;
DOI:10.1002/ejoc.201200919

Reference yield:

: 1350922-83-6
(R)-benzyl [6-(1,3-dioxoisoindolin-2-yl)-4-oxo-hexan-2-yl]carbamate

: 1419075-35-6
C₂₆H₂₈N₂O₄

Guidance literature:: Multi-step reaction with 11 steps

1.1: toluene-4-sulfonic acid; trimethyl orthoformate / dichloromethane / 20 °C

2.1: hydrazine hydrate / methanol / 2 h / Reflux

3.1: dmap; triethylamine / dichloromethane / 0 - 20 °C

3.2: 0.5 h / 0 - 20 °C

4.1: palladium 10% on activated carbon; ammonium formate / methanol / 3 h / Reflux

5.1: magnesium sulfate / dichloromethane / Reflux

5.2: 14 h / 40 °C

6.1: palladium 10% on activated carbon; ammonium formate / methanol / 2 h / Reflux

7.1: sodium carbonate / dichloromethane; water / 3 h / 20 °C

8.1: Amberlite IRA 401 / methanol

9.1: triethylamine / toluene / 3 h / Dean-Stark; Reflux

10.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 1.5 h / -20 - 5 °C / Inert atmosphere

11.1: methanesulfonic acid / dichloromethane / 1.5 h / Inert atmosphere

With dmap; sodium tetrahydroborate; methanesulfonic acid; palladium 10% on activated carbon; ammonium formate; sodium carbonate; magnesium sulfate; toluene-4-sulfonic acid; hydrazine hydrate; triethylamine; trimethyl orthoformate; In tetrahydrofuran; methanol; dichloromethane; water; toluene; 5.1: |Mannich Aminomethylation;
DOI:10.1002/ejoc.201200919