6-(4-bromophenylamino)-4-chloronicotinonitrile

Base Information

Chemical Name:6-(4-bromophenylamino)-4-chloronicotinonitrile
CAS No.:1337906-09-8
Molecular Formula:C₁₂H₇BrClN₃
Molecular Weight:308.565
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-(4-bromophenylamino)-4-chloronicotinonitrile

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Technology Process of 6-(4-bromophenylamino)-4-chloronicotinonitrile

There total 2 articles about 6-(4-bromophenylamino)-4-chloronicotinonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₄H₉BrClN₃O

: 1337906-09-8
6-(4-bromophenylamino)-4-chloronicotinonitrile

Guidance literature:: With water; lithium hydroxide; In 1,4-dioxane; at 20 ℃; for 0.5h; Inert atmosphere; Sealed microwave vial;
DOI:10.1055/s-0030-1260080

Reference yield:

: 166526-03-0
4,6-dichloropyridine-3-carbonitrile

: 103-88-8
4-bromoacetanilide

: 1337906-09-8
6-(4-bromophenylamino)-4-chloronicotinonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: palladium diacetate; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / 1,4-dioxane / 4 h / 90 °C / Sealed microwave vial; Inert atmosphere

2: water; lithium hydroxide / 1,4-dioxane / 0.5 h / 20 °C / Inert atmosphere; Sealed microwave vial

With water; palladium diacetate; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; lithium hydroxide; In 1,4-dioxane;
DOI:10.1055/s-0030-1260080