ferrocenecarboxaldehyde 2,4-dichlorobenzoylhydrazone

Base Information

Chemical Name:ferrocenecarboxaldehyde 2,4-dichlorobenzoylhydrazone
CAS No.:357164-96-6
Molecular Formula:C₁₈H₁₄Cl₂FeN₂O
Molecular Weight:401.075
Hs Code.:

Synonyms:

Suppliers and Price of ferrocenecarboxaldehyde 2,4-dichlorobenzoylhydrazone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of ferrocenecarboxaldehyde 2,4-dichlorobenzoylhydrazone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of ferrocenecarboxaldehyde 2,4-dichlorobenzoylhydrazone

There total 1 articles about ferrocenecarboxaldehyde 2,4-dichlorobenzoylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 12093-10-6
ferrocenecarboxaldehyde

: 5814-06-2
2,4-dichlorobenzohydrazide

: 357164-96-6
ferrocenecarboxaldehyde 2,4-dichlorobenzoylhydrazone

Guidance literature:: In ethanol; Fe-compd. in EtOH was added to EtOH soln. of Cl-compd., stirring and refluxing for 2 h; mixt. was cooled to room temp., ppt. was filtered, washed twice with EtOH and Et2O, recrystd. from anhyd. EtOH, dried in vac.;
DOI:10.1081/SIM-100002048

Reference yield: 82.0%

: cobalt(II) acetate hydrate

: 357164-96-6
ferrocenecarboxaldehyde 2,4-dichlorobenzoylhydrazone

: 356583-51-2
bis(ferrocenecarboxaldehyde 2,4-dichlorobenzoylhydrazonato)cobalt

Guidance literature:: In ethanol; 0.5 equiv. of metal salt was dissolved in ethanol at 50 °C, this soln. was added to EtOH soln. of Fe-compd. at room temp., stirring for 20 min at this temp., reflux for 6-8 h; solid was collected, washed twice with warm EtOH and Et2O, dried in vac., elem. anal.;
DOI:10.1081/SIM-100002048

Reference yield: 82.0%

: nickel(II) acetate hydrate

: 357164-96-6
ferrocenecarboxaldehyde 2,4-dichlorobenzoylhydrazone

: 356583-52-3
bis(ferrocenecarboxaldehyde 2,4-dichlorobenzoylhydrazonato)nickel

Guidance literature:: In ethanol; 0.5 equiv. of metal salt was dissolved in ethanol at 50 °C, this soln. was added to EtOH soln. of Fe-compd. at room temp., stirring for 20 min at this temp., reflux for 6-8 h; solid was collected, washed twice with warm EtOH and Et2O, dried in vac., elem. anal.;
DOI:10.1081/SIM-100002048