C₃₀H₃₀N₂O₈

Base Information

Chemical Name:C₃₀H₃₀N₂O₈
CAS No.:1408237-00-2
Molecular Formula:C₃₀H₃₀N₂O₈
Molecular Weight:546.577
Hs Code.:

C<sub>30</sub>H<sub>30</sub>N<sub>2</sub>O<sub>8</sub>

Synonyms:

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Chemical Property of C₃₀H₃₀N₂O₈

Chemical Property:

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Technology Process of C₃₀H₃₀N₂O₈

There total 9 articles about C₃₀H₃₀N₂O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1408236-94-1
C₂₁H₂₇NO₇

: 1408237-00-2
C₃₀H₃₀N₂O₈

Guidance literature:: Multi-step reaction with 12 steps

1.1: triethylamine / dichloromethane / 2 h / 0 °C

2.1: caesium carbonate / N,N-dimethyl-formamide / 20 h / 100 °C

3.1: potassium hydroxide / water; ethanol / 2 h / 120 °C

3.2: 4 h / 20 °C

4.1: dimethylsulfide borane complex / tetrahydrofuran / 12 h / 0 °C

5.1: iodine; potassium carbonate / methanol; water / 24 h / 20 °C

6.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / benzene / 2 h / 90 °C

7.1: tri-n-butyl-tin hydride; Dess-Martin periodane / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

8.1: potassium carbonate / methanol / 2 h / 0 - 20 °C / Inert atmosphere

9.1: triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(II) sulfate; sodium L-ascorbate / N,N-dimethyl-formamide / 5 h / 80 °C / Inert atmosphere

10.1: sodium tetrachloroaurate(III) dihyrate / ethanol / 4 h / 20 °C / Inert atmosphere

11.1: tetrahydrofuran / 0 - 20 °C / Inert atmosphere

12.1: 40 h

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium tetrachloroaurate(III) dihyrate; 2,2'-azobis(isobutyronitrile); dimethylsulfide borane complex; iodine; tri-n-butyl-tin hydride; potassium carbonate; caesium carbonate; Dess-Martin periodane; copper(II) sulfate; sodium L-ascorbate; triethylamine; potassium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; benzene; 8.1: |Seyferth-Gilbert Homologation / 9.1: |Sonogashira Cross-Coupling;
DOI:10.1021/ol3027945

Reference yield:

: 1408236-88-3
C₂₁H₂₅NO₆

: 1408237-00-2
C₃₀H₃₀N₂O₈

Guidance literature:: Multi-step reaction with 10 steps

1.1: potassium hydroxide / water; ethanol / 2 h / 120 °C

1.2: 4 h / 20 °C

2.1: dimethylsulfide borane complex / tetrahydrofuran / 12 h / 0 °C

3.1: iodine; potassium carbonate / methanol; water / 24 h / 20 °C

4.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / benzene / 2 h / 90 °C

5.1: tri-n-butyl-tin hydride; Dess-Martin periodane / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

6.1: potassium carbonate / methanol / 2 h / 0 - 20 °C / Inert atmosphere

7.1: triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(II) sulfate; sodium L-ascorbate / N,N-dimethyl-formamide / 5 h / 80 °C / Inert atmosphere

8.1: sodium tetrachloroaurate(III) dihyrate / ethanol / 4 h / 20 °C / Inert atmosphere

9.1: tetrahydrofuran / 0 - 20 °C / Inert atmosphere

10.1: 40 h

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium tetrachloroaurate(III) dihyrate; 2,2'-azobis(isobutyronitrile); dimethylsulfide borane complex; iodine; tri-n-butyl-tin hydride; potassium carbonate; Dess-Martin periodane; copper(II) sulfate; sodium L-ascorbate; triethylamine; potassium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; benzene; 6.1: |Seyferth-Gilbert Homologation / 7.1: |Sonogashira Cross-Coupling;
DOI:10.1021/ol3027945

Reference yield:

: C₁₉H₂₁NO₅

: 1408237-00-2
C₃₀H₃₀N₂O₈

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate / methanol / 2 h / 0 - 20 °C / Inert atmosphere

2: triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(II) sulfate; sodium L-ascorbate / N,N-dimethyl-formamide / 5 h / 80 °C / Inert atmosphere

3: sodium tetrachloroaurate(III) dihyrate / ethanol / 4 h / 20 °C / Inert atmosphere

4: tetrahydrofuran / 0 - 20 °C / Inert atmosphere

5: 40 h

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium tetrachloroaurate(III) dihyrate; potassium carbonate; copper(II) sulfate; sodium L-ascorbate; triethylamine; In tetrahydrofuran; methanol; ethanol; N,N-dimethyl-formamide; 1: |Seyferth-Gilbert Homologation / 2: |Sonogashira Cross-Coupling;
DOI:10.1021/ol3027945