(dicyclohexylphosphino) cobaltocenium hexafluorophosphate

Base Information

Chemical Name:(dicyclohexylphosphino) cobaltocenium hexafluorophosphate
CAS No.:917225-51-5
Molecular Formula:C₂₂H₃₁CoP*F₆P
Molecular Weight:530.419
Hs Code.:

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Chemical Property of (dicyclohexylphosphino) cobaltocenium hexafluorophosphate

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Technology Process of (dicyclohexylphosphino) cobaltocenium hexafluorophosphate

There total 1 articles about (dicyclohexylphosphino) cobaltocenium hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: ammonium hexafluorophosphate

: 67-72-1
hexachloroethane

: sodium cyclopentadienide

: 7646-79-9,14543-09-0,16413-89-1
cobalt(II) chloride

: 16523-54-9
chlorodicyclohexylphosphane

: 917225-51-5
(dicyclohexylphosphino) cobaltocenium hexafluorophosphate

: 915955-74-7
1,1'-bis(dicyclohexylphosphino) cobaltocenium hexafluorophosphate

Guidance literature:: With n-C₄H₉Li; In tetrahydrofuran; diethyl ether; hexane; byproducts: LiCl; (N2); using Schlenk techniques; mixing ClPCy2/ether and NaCp/THF at -30°C; stirring for 1.5 h at r.t.; addn. n-BuLi/C6H14 at -78°C; stirring for 1.5 h at r.t.; addn. of CoCl2; reflux overnight; stirringwith C2Cl6; drying, addn. aq. NH4PF6; addn. to H2O; extn. with CH2Cl2; drying of combined org. layer over MgSO4; filtration, evapn. of solvent in vac., chromy. (silica gel, CH2Cl2); elem. anal.;
DOI:10.1016/j.jorganchem.2007.05.046