N-<<2-<2-<2-(3-dimethylaminopropylcarbamoyl)-1-methyl-4-pyrrolyl>carbamoyl-1-methyl-4-pyrrolyl>carbamoylethyl>>-2-nitro-3-hydroxy-4-methylbenzamide trifluoroacetate

Base Information

Chemical Name:N-<<2-<2-<2-(3-dimethylaminopropylcarbamoyl)-1-methyl-4-pyrrolyl>carbamoyl-1-methyl-4-pyrrolyl>carbamoylethyl>>-2-nitro-3-hydroxy-4-methylbenzamide trifluoroacetate
CAS No.:87590-31-6
Molecular Formula:C₂HF₃O₂*C₂₈H₃₆N₈O₇
Molecular Weight:710.667
Hs Code.:

N-<<2-<2-<2-(3-dimethylaminopropylcarbamoyl)-1-methyl-4-pyrrolyl>carbamoyl-1-methyl-4-pyrrolyl>carbamoylethyl>>-2-nitro-3-hydroxy-4-methylbenzamide trifluoroacetate

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Chemical Property of N-<<2-<2-<2-(3-dimethylaminopropylcarbamoyl)-1-methyl-4-pyrrolyl>carbamoyl-1-methyl-4-pyrrolyl>carbamoylethyl>>-2-nitro-3-hydroxy-4-methylbenzamide trifluoroacetate

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Technology Process of N-<<2-<2-<2-(3-dimethylaminopropylcarbamoyl)-1-methyl-4-pyrrolyl>carbamoyl-1-methyl-4-pyrrolyl>carbamoylethyl>>-2-nitro-3-hydroxy-4-methylbenzamide trifluoroacetate

There total 5 articles about N-<<2-<2-<2-(3-dimethylaminopropylcarbamoyl)-1-methyl-4-pyrrolyl>carbamoyl-1-methyl-4-pyrrolyl>carbamoylethyl>>-2-nitro-3-hydroxy-4-methylbenzamide trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7536-35-8
2-nitro-3-benzyloxy-4-methylbenzoyl chloride

: 87590-31-6
N-<<2-<2-<2-(3-dimethylaminopropylcarbamoyl)-1-methyl-4-pyrrolyl>carbamoyl-1-methyl-4-pyrrolyl>carbamoylethyl>>-2-nitro-3-hydroxy-4-methylbenzamide trifluoroacetate

Guidance literature:: Multi-step reaction with 4 steps

1: 85.5 percent / triethylamine / CHCl₃

2: 62 percent / hydrazine hydrate / ethanol

3: aq. HCl, CH₃COOH, NaNO₂ / 0.25 h / 0 °C

4: CHCl₃; dioxane / Ambient temperature

With hydrogenchloride; hydrazine hydrate; acetic acid; triethylamine; sodium nitrite; In 1,4-dioxane; ethanol; chloroform;

Reference yield:

: 87590-25-8
N-(2-ethoxycarbonylethyl)-2-nitro-3-benzyloxy-4-methylbenzamide

: 87590-31-6
N-<<2-<2-<2-(3-dimethylaminopropylcarbamoyl)-1-methyl-4-pyrrolyl>carbamoyl-1-methyl-4-pyrrolyl>carbamoylethyl>>-2-nitro-3-hydroxy-4-methylbenzamide trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1: 62 percent / hydrazine hydrate / ethanol

2: aq. HCl, CH₃COOH, NaNO₂ / 0.25 h / 0 °C

3: CHCl₃; dioxane / Ambient temperature

With hydrogenchloride; hydrazine hydrate; acetic acid; sodium nitrite; In 1,4-dioxane; ethanol; chloroform;

Reference yield:

: 65361-31-1
N-[3-(dimethylamino)propyl]-1-methyl-4-{[(1-methyl-4-nitro-1H-pyrrol-2-yl)carbonyl]amino}-1H-pyrrole-2-carboxamide

: 87590-31-6
N-<<2-<2-<2-(3-dimethylaminopropylcarbamoyl)-1-methyl-4-pyrrolyl>carbamoyl-1-methyl-4-pyrrolyl>carbamoylethyl>>-2-nitro-3-hydroxy-4-methylbenzamide trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: H₂

2: CHCl₃; dioxane / Ambient temperature

With hydrogen; In 1,4-dioxane; chloroform;