Cu(tris(3-phenylpyrazolyl)methane sulfonate)(2,6-dimethylphenyl isocyanide)

Base Information

• Chemical Name: Cu(tris(3-phenylpyrazolyl)methane sulfonate)(2,6-dimethylphenyl isocyanide)
• CAS No.: 1391853-76-1
• Molecular Formula: C₃₇H₃₀CuN₇O₃S
• Molecular Weight: 716.302
• Mol file: 1391853-76-1.mol

Synonyms:

Chemical Property of Cu(tris(3-phenylpyrazolyl)methane sulfonate)(2,6-dimethylphenyl isocyanide)

Chemical Property:

Purity/Quality:

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Useful:

Technology Process of Cu(tris(3-phenylpyrazolyl)methane sulfonate)(2,6-dimethylphenyl isocyanide)

There total 1 articles about Cu(tris(3-phenylpyrazolyl)methane sulfonate)(2,6-dimethylphenyl isocyanide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

[Cu(tris(3-phenylpyrazolyl)methanesulfonate-N,N,O)(acetonitrile)] (1073256-35-5) + 2,6-dimethylphenyl isonitrile (119072-54-7,2769-71-3) → Cu(tris(3-phenylpyrazolyl)methane sulfonate)(2,6-dimethylphenyl isocyanide) (1391853-76-1)

Guidance literature:

In methanol; under N2; to MeOH soln. of Cu compd. isocyanide added slowly, stirred overnight; elem. anal.;

DOI:10.1016/j.jorganchem.2012.03.022

Reference yield: 84.0%

Cu(tris(3-phenylpyrazolyl)methane sulfonate)(2,6-dimethylphenyl isocyanide) (1391853-76-1) + 3-iminoisoindolinone (14352-51-3) → Cu(tris(3-phenylpyrazolyl)methane sulfonate)(3-iminoisoindolin-1-one)

Guidance literature:

In chloroform; under N2; solid 3-iminoisoindolin-1-one added to CHCl3 soln. of Cu compd., suspn. refluxed overnight, left for 1 h; filtered, filtrate evapd.. powder washed (Et2O), dried (vac., 20-25°C; elem. anal.;

DOI:10.1016/j.jorganchem.2012.03.022

upstream raw materials:

[Cu(tris(3-phenylpyrazolyl)methanesulfonate-N,N,O)(acetonitrile)]

2,6-dimethylphenyl isonitrile