C₂₆H₂₈N₂O₃

Base Information

• Chemical Name: C₂₆H₂₈N₂O₃
• CAS No.: 130253-44-0
• Molecular Formula: C₂₆H₂₈N₂O₃
• Molecular Weight: 416.52
• Mol file: 130253-44-0.mol

Synonyms:

Chemical Property of C₂₆H₂₈N₂O₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₆H₂₈N₂O₃

There total 13 articles about C₂₆H₂₈N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C32H44N2O4Si (130253-43-9) → C26H28N2O3 (130253-44-0)

Guidance literature:

Multi-step reaction with 4 steps

1: 93 percent / Et₃N, DMAP / CH₂Cl₂

2: 66 percent / H₂ / Pd-C / acetic acid; ethanol

3: 90 percent / n-Bu₄NF / tetrahydrofuran

4: MgO / H₂O; tetrahydrofuran

With dmap; tetrabutyl ammonium fluoride; hydrogen; magnesium oxide; triethylamine; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane; water; acetic acid;

DOI:10.1016/S0040-4039(00)88787-0

Reference yield:

C29H34N2O5 (130278-17-0) → C26H28N2O3 (130253-44-0)

Guidance literature:

Multi-step reaction with 10 steps

1: 90 percent / CH₂Cl₂

2: 68 percent / Pb(OAc)4 / CH₂Cl₂ / -70 °C

3: AcOH / tetrahydrofuran; H₂O / Ambient temperature

4: 80 percent / NaBH₄ / methanol / 0 °C

5: 80 percent / Et₃N / CH₂Cl₂

6: 90 percent / aq. KOH / methanol

7: 93 percent / Et₃N, DMAP / CH₂Cl₂

8: 66 percent / H₂ / Pd-C / acetic acid; ethanol

9: 90 percent / n-Bu₄NF / tetrahydrofuran

10: MgO / H₂O; tetrahydrofuran

With lead(IV) acetate; dmap; potassium hydroxide; sodium tetrahydroborate; tetrabutyl ammonium fluoride; hydrogen; magnesium oxide; acetic acid; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; acetic acid;

DOI:10.1016/S0040-4039(00)88787-0

Reference yield:

C28H32N2O5 (130253-36-0) → C26H28N2O3 (130253-44-0)

Guidance literature:

Multi-step reaction with 6 steps

1: 80 percent / Et₃N / CH₂Cl₂

2: 90 percent / aq. KOH / methanol

3: 93 percent / Et₃N, DMAP / CH₂Cl₂

4: 66 percent / H₂ / Pd-C / acetic acid; ethanol

5: 90 percent / n-Bu₄NF / tetrahydrofuran

6: MgO / H₂O; tetrahydrofuran

With dmap; potassium hydroxide; tetrabutyl ammonium fluoride; hydrogen; magnesium oxide; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; acetic acid;

DOI:10.1016/S0040-4039(00)88787-0

upstream raw materials:

C₂₄H₃₆N₂OSi

C₂₈H₃₂N₂O₅

C₃₂H₄₄N₂O₄Si

C₂₉H₃₄N₂O₅