1,2-cis-1-(p-acetoxyphenyl)-5-methoxy-2-phenylindane

Base Information

Chemical Name:1,2-cis-1-(p-acetoxyphenyl)-5-methoxy-2-phenylindane
CAS No.:78014-10-5
Molecular Formula:C₂₄H₂₂O₃
Molecular Weight:358.437
Hs Code.:

Synonyms:

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Chemical Property of 1,2-cis-1-(p-acetoxyphenyl)-5-methoxy-2-phenylindane

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Technology Process of 1,2-cis-1-(p-acetoxyphenyl)-5-methoxy-2-phenylindane

There total 16 articles about 1,2-cis-1-(p-acetoxyphenyl)-5-methoxy-2-phenylindane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 108-24-7
acetic anhydride

: 78014-08-1,118848-49-0
1,2-trans-1-(p-hydroxyphenyl)-5-methoxy-2-phenylindane

: 78014-10-5,124521-65-9
1,2-trans-1-(p-acetoxyphenyl)-5-methoxy-2-phenylindane

Guidance literature:: With pyridine;

Reference yield: 84.0%

: 108-24-7
acetic anhydride

: 78014-08-1,118848-49-0
1,2-cis-1-(p-hydroxyphenyl)-5-methoxy-2-phenylindane

: 78014-10-5,124521-65-9
1,2-cis-1-(p-acetoxyphenyl)-5-methoxy-2-phenylindane

Guidance literature:: With pyridine;
DOI:10.1016/0223-5234(89)90115-3

Reference yield:

: 103-82-2
phenylacetic acid

: 78014-10-5,124521-65-9
1,2-trans-1-(p-acetoxyphenyl)-5-methoxy-2-phenylindane

Guidance literature:: Multi-step reaction with 7 steps

1: polyphosphoric acid / 0.5 h / Heating

2: 35 percent / NaOMe / 4 h / Heating

3: 95 percent / hydrogen / 10 percent Pd-C / ethyl acetate

4: 45 percent / anhydrous AlCl₃ / benzene / 3.5 h / Heating

5: 90 percent / LiAlH₄ / tetrahydrofuran / 2 h / Ambient temperature

6: 58 percent / p-TsOH / benzene / 2 h / Heating

7: 90 percent / pyridine

With pyridine; lithium aluminium tetrahydride; aluminium trichloride; PPA; hydrogen; sodium methylate; toluene-4-sulfonic acid; palladium on activated charcoal; In tetrahydrofuran; ethyl acetate; benzene;
DOI:10.1016/0223-5234(89)90115-3