3-diphenylphosphino-(1R)-(+)-camphor dimethylhydrazone

Base Information

Chemical Name:3-diphenylphosphino-(1R)-(+)-camphor dimethylhydrazone
CAS No.:135707-31-2
Molecular Formula:C₂₄H₃₁N₂P
Molecular Weight:378.497
Hs Code.:

Synonyms:

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Chemical Property of 3-diphenylphosphino-(1R)-(+)-camphor dimethylhydrazone

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Technology Process of 3-diphenylphosphino-(1R)-(+)-camphor dimethylhydrazone

There total 2 articles about 3-diphenylphosphino-(1R)-(+)-camphor dimethylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 464-49-3,68546-28-1
(1R,4R)-1,7,7-trimethylbicyclo[2.2.1]heptan-2-one

: 135707-31-2,141610-85-7
3-diphenylphosphino-(1R)-(+)-camphor dimethylhydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / acetic acid / ethanol / 43 h / Heating

2: 1) LiBu / 1) hexane, THF, -15 deg C, 35 min 2) THF, -15 deg C to r.t.

With n-butyllithium; acetic acid; In ethanol;
DOI:10.1039/DT9910001183

Reference yield:

: 111537-61-2
(1R)-(+)-camphor dimethylhydrazone

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 135707-31-2,141610-85-7
3-diphenylphosphino-(1R)-(+)-camphor dimethylhydrazone

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1) hexane, THF, -15 deg C, 35 min 2) THF, -15 deg C to r.t.;
DOI:10.1039/DT9910001183

Reference yield: 90.0%

: 14220-64-5,15617-18-2,39958-10-6
cis-dichlorobis(benzonitrile)palladium(II)

: 135707-31-2,141610-85-7
3-diphenylphosphino-(1R)-(+)-camphor dimethylhydrazone

: PdCl₂(P(C₆H₅)2C₁₀H₁₅NN(CH₃)2)

Guidance literature:: In dichloromethane; addn. of exo-phosphine in CH2Cl2 to soln. of Pd-complex in CH2Cl2, yellow soln., addn. of EtOH, pptn.; elem. anal.;;
DOI:10.1039/DT9920000999