2,9-diphenyl-5,13;6,12-dietheno-5a,12a-[2]oxapropano-[1,2,4]triazolo[1,2-a][1,2,4]triazolo[1',2':1,2]pyridazino[4,5-d]pyridazine-1,3,8,10-tetraone

Base Information

• Chemical Name: 2,9-diphenyl-5,13;6,12-dietheno-5a,12a-[2]oxapropano-[1,2,4]triazolo[1,2-a][1,2,4]triazolo[1',2':1,2]pyridazino[4,5-d]pyridazine-1,3,8,10-tetraone
• CAS No.: 36843-48-8
• Molecular Formula: C₂₈H₂₂N₆O₅
• Molecular Weight: 522.52
• Mol file: 36843-48-8.mol

Synonyms:

Chemical Property of 2,9-diphenyl-5,13;6,12-dietheno-5a,12a-[2]oxapropano-[1,2,4]triazolo[1,2-a][1,2,4]triazolo[1',2':1,2]pyridazino[4,5-d]pyridazine-1,3,8,10-tetraone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,9-diphenyl-5,13;6,12-dietheno-5a,12a-[2]oxapropano-[1,2,4]triazolo[1,2-a][1,2,4]triazolo[1',2':1,2]pyridazino[4,5-d]pyridazine-1,3,8,10-tetraone

There total 2 articles about 2,9-diphenyl-5,13;6,12-dietheno-5a,12a-[2]oxapropano-[1,2,4]triazolo[1,2-a][1,2,4]triazolo[1',2':1,2]pyridazino[4,5-d]pyridazine-1,3,8,10-tetraone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-Phenyl-1,2,4-triazolidine-3,5-dione (4233-33-4) + 2-phenyl-5r,10c-etheno-5at,9at-[2]oxapropano-[1,2,4]triazolo[1,2-b]phthalazine-1,3-dione (36843-47-7,36843-49-9) → 2,9-diphenyl-5r,13c;6c,12c-dietheno-5at,12at-[2]oxapropano-[1,2,4]triazolo[1,2-a][1,2,4]triazolo[1',2':1,2]pyridazino[4,5-d]pyridazine-1,3,8,10-tetraone (36843-48-8,36843-50-2)

Guidance literature:

In acetone; Ambient temperature;

DOI:10.1016/S0040-4020(01)93575-6

Reference yield:

4-Phenyl-1,2,4-triazolidine-3,5-dione (4233-33-4) + 12-oxa-[4.4.3]propella-2,4,7,9-tetraene → 2,9-diphenyl-5r,13c;6c,12c-dietheno-5at,12at-[2]oxapropano-[1,2,4]triazolo[1,2-a][1,2,4]triazolo[1',2':1,2]pyridazino[4,5-d]pyridazine-1,3,8,10-tetraone (36843-48-8,36843-50-2)

Guidance literature:

In dichloromethane; Ambient temperature;

DOI:10.1016/S0040-4020(01)93575-6

Reference yield:

2,9-diphenyl-5r,13c;6c,12c-dietheno-5at,12at-[2]oxapropano-[1,2,4]triazolo[1,2-a][1,2,4]triazolo[1',2':1,2]pyridazino[4,5-d]pyridazine-1,3,8,10-tetraone (36843-48-8,36843-50-2) → 2,9-dicyclohexyl-5r,13c;6c,12c-diethano-5at,12at-[2]oxapropano-[1,2,4]triazolo[1,2-a][1,2,4]triazolo[1',2':1,2]pyridazino[4,5-d]pyridazine-1,3,8,10-tetraone (51334-89-5)

Guidance literature:

With hydrogen; platinum(IV) oxide; In acetic acid; for 20h; Ambient temperature;

DOI:10.1016/S0040-4020(01)93365-4

upstream raw materials:

4-Phenyl-1,2,4-triazolidine-3,5-dione

2-phenyl-5r,10c-etheno-5at,9at-[2]oxapropano-[1,2,4]triazolo[1,2-b]phthalazine-1,3-dione

Downstream raw materials:

3,7-diphenyl-octahydro-1b,3,4a,5b,7,8a-hexaaza-1,5-cyclo-1,5-[2]oxapropano-tetracyclopenta[b,def,h,jkl]biphenylene-2,4,6,8-tetraone

2,9-dicyclohexyl-5r,13c;6c,12c-diethano-5at,12at-[2]oxapropano-[1,2,4]triazolo[1,2-a][1,2,4]triazolo[1',2':1,2]pyridazino[4,5-d]pyridazine-1,3,8,10-tetraone

2,9-diphenyl-5r,13c;6t,12t-diethano-5ac,12ac-[2]oxapropano-[1,2,4]triazolo[1,2-a][1,2,4]triazolo[1',2':1,2]pyridazino[4,5-d]pyridazine-1,3,8,10-tetraone