Hexacyclo[7:2:1:0(2,5):0(3,10):0(4,8):0(6,12)]dodacane

Base Information

• Chemical Name: Hexacyclo[7:2:1:0(2,5):0(3,10):0(4,8):0(6,12)]dodacane
• CAS No.: 704-02-9
• Molecular Formula: C₁₂H₁₄
• Molecular Weight: 158.243
• DSSTox Substance ID: DTXSID301199756
• Nikkaji Number: J1.026.628I
• Mol file: 704-02-9.mol

Synonyms:704-02-9;Hexacyclo[7:2:1:0(2,5):0(3,10):0(4,8):0(6,12)]dodacane;Hexacyclo(7:2:1:0(2,5):0(3,10):0(4,8):0(6,12))dodacane;DTXSID301199756;Decahydro-1,5,2,4-ethanediylidenecyclopenta[cd]pentalene;1,5,2,4-Ethanediylidenecyclopenta[cd]pentalene, decahydro-

Chemical Property of Hexacyclo[7:2:1:0(2,5):0(3,10):0(4,8):0(6,12)]dodacane

Chemical Property:

• Vapor Pressure: 0.104mmHg at 25°C
• Boiling Point: 229.6°C at 760 mmHg
• Flash Point: 69°C
• Density: 1.341g/cm³
• XLogP3: 2.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 0
• Exact Mass: 158.109550447
• Heavy Atom Count: 12
• Complexity: 260

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1C2C3C4CC5C3C1C6C2C4C56

Technology Process of Hexacyclo[7:2:1:0(2,5):0(3,10):0(4,8):0(6,12)]dodacane

There total 10 articles about Hexacyclo[7:2:1:0(2,5):0(3,10):0(4,8):0(6,12)]dodacane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

C13H14O2 (101418-79-5) → 1,3-bishomopentaprismane (704-02-9)

Guidance literature:

at 700 ℃; under 0.01 Torr;

DOI:10.1021/jo00360a046

Reference yield:

1,8,9,10,11,11-Hexachlor-hexacyclo[6.2.1.13.6.02.7.04.10.05.9]dodecan (3212-28-0) → 1,3-bishomopentaprismane (704-02-9)

Guidance literature:

With lithium; In tetrahydrofuran; tert-butyl alcohol;

DOI:10.1021/jo00422a022

Reference yield:

(1α,4α,4aα,5α,8α,8aα)-1,4,4a,5,8,8a-hexahydro-1,4:5,8-dimethanonaphthalene (1076-13-7) → C12H14 (704-02-9)

Guidance literature:

With 9,10-Dicyanoanthracene; In cyclohexane; at 25 ℃; Quantum yield; Rate constant; Mechanism; Irradiation; other sensitizer, other solvent; quenching constants; isomerization on direct photolysis and with triplet sensitizers, via fluorescence quenching, and on irradiation of charge-transfer complexes;;

DOI:10.1021/ja00343a032

upstream raw materials:

1,8,9,10,11,11-Hexachlor-hexacyclo[6.2.1.1^3.6.0^2.7.0^4.10.0^5.9]dodecan

11-methylenepentacyclo<5.4.0.0^2,6.0^3,10.0^5,9>undecane-8-spiro-3'-diazirine

C₁₉H₁₉N₂O₂S^(1-)*Na⁽¹⁺⁾

C₁₃H₁₄O₂

Downstream raw materials:

acs-Tetracyclo<7.2.1.0^4,11.0^6,10>dodeca-2,7-dien

2a,3,3a,5a,6,6a,6b,6c-Octahydro-dicyclopenta[cd,gh]pentalene