Olean-11-ene-3,16-diol,13,28-epoxy-, (3b,16a)- (9CI)

Base Information

• Chemical Name: Olean-11-ene-3,16-diol,13,28-epoxy-, (3b,16a)- (9CI)
• CAS No.: 79786-12-2
• Molecular Formula: C30H48 O3
• Molecular Weight: 456.709
• Mol file: 79786-12-2.mol

Synonyms:2H,5H-14a,4a-(Epoxymethano)picene,olean-11-ene-3,16-diol deriv.; Rotundiogenin A

Chemical Property of Olean-11-ene-3,16-diol,13,28-epoxy-, (3b,16a)- (9CI)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Olean-11-ene-3,16-diol,13,28-epoxy-, (3b,16a)- (9CI)

There total 4 articles about Olean-11-ene-3,16-diol,13,28-epoxy-, (3b,16a)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.4%

saikosaponin c → saikogenin E (13715-23-6,79786-12-2) + prosapogenin E3 + prosapogenin E2 + prosapogenin E1

Guidance literature:

With sodium; In ethanol; for 36h; Ambient temperature;

DOI:10.1039/c39860001417

Reference yield:

saikosaponin c → prosaikosaponin E-3 (106452-35-1) + prosaikogenin E-2 + prosaikogenin E-1 + saikogenin E (13715-23-6,79786-12-2)

Guidance literature:

With sodium; In butan-1-ol; at 80 ℃; for 6h;

Reference yield:

Corchorusin D (108886-04-0) → saikogenin E (13715-23-6,79786-12-2)

Guidance literature:

With potassium hydroxide; sodium periodate; Yield given. Multistep reaction; 1.) 95 percent EtOH, water, RT, overnight; 2.) 85 percent EtOH, 1 h, reflux;

upstream raw materials:

Corchorusin D

Downstream raw materials:

primulagenin A