C₃₄H₃₉F₁₂N₃O₉

Base Information

• Chemical Name: C₃₄H₃₉F₁₂N₃O₉
• CAS No.: 1315482-65-5
• Molecular Formula: C₃₄H₃₉F₁₂N₃O₉
• Molecular Weight: 861.679
• Mol file: 1315482-65-5.mol

Synonyms:

Chemical Property of C₃₄H₃₉F₁₂N₃O₉

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₄H₃₉F₁₂N₃O₉

There total 5 articles about C₃₄H₃₉F₁₂N₃O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C39H47F12N3O11 (1315482-64-4) → C34H39F12N3O9 (1315482-65-5)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1021/ja203996c

Reference yield:

tert-butyl N-[2-[2-[2-[2-(2-aminoethoxy)ethoxy]ethoxy]ethoxy]ethyl]carbamate (811442-84-9) → C34H39F12N3O9 (1315482-65-5)

Guidance literature:

Multi-step reaction with 4 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / -10 °C / Inert atmosphere

2: N,N-dimethyl-formamide / 5 h / 20 °C / Inert atmosphere

3: dmap / dichloromethane / 5 h / 20 °C / Inert atmosphere

4: trifluoroacetic acid / dichloromethane / 2 h / 20 °C

With dmap; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1021/ja203996c

Reference yield:

C17H33BrN2O7 (1315482-62-2) → C34H39F12N3O9 (1315482-65-5)

Guidance literature:

Multi-step reaction with 3 steps

1: N,N-dimethyl-formamide / 5 h / 20 °C / Inert atmosphere

2: dmap / dichloromethane / 5 h / 20 °C / Inert atmosphere

3: trifluoroacetic acid / dichloromethane / 2 h / 20 °C

With dmap; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1021/ja203996c

upstream raw materials:

tert-butyl N-[2-[2-[2-[2-(2-aminoethoxy)ethoxy]ethoxy]ethoxy]ethyl]carbamate

C₁₇H₃₃BrN₂O₇

C₂₁H₄₃N₃O₉

C₃₉H₄₇F₁₂N₃O₁₁

Downstream raw materials:

C₄₁H₄₄F₁₂N₄O₁₂S

Refernces