(12R)-(2,2,3,3,12-2H5)myristic acid

Base Information

Chemical Name:(12R)-(2,2,3,3,12-2H5)myristic acid
CAS No.:199013-53-1
Molecular Formula:C₁₄H₂₈O₂
Molecular Weight:233.335
Hs Code.:

Synonyms:

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Chemical Property of (12R)-(2,2,3,3,12-2H5)myristic acid

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Technology Process of (12R)-(2,2,3,3,12-2H5)myristic acid

There total 5 articles about (12R)-(2,2,3,3,12-2H5)myristic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 199013-49-5
C₁₃H₂₂⁽²⁾H₄O₃

: 199013-53-1,358730-97-9
(12R)-(2,2,3,3,12-2H5)myristic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / (CO)2Cl₂ / dimethylsulfoxide; triethylamine

2: 89 percent / Ti(i-PrO)4, (1S,2S)-1,2-N,N'-bis(trifluoromethylsulfonylamino)cyclohexane / toluene

3: 72 percent / pyridine

4: 1.) LiAlD₄, 2.) CrO₃, H₂SO₄ / 1.) Et₂O, 2.) H₂O

With chromium(VI) oxide; titanium(IV) isopropylate; lithium aluminium deuteride; oxalyl dichloride; sulfuric acid; C,C,C-trifluoro-N-(2-trifluoromethanesulfonylaminocyclohexyl)methanesulfonamide; In pyridine; dimethyl sulfoxide; triethylamine; toluene;
DOI:10.1021/ja972577v

Reference yield:

: 199013-50-8
C₁₃H₂₀⁽²⁾H₄O₃

: 199013-53-1,358730-97-9
(12R)-(2,2,3,3,12-2H5)myristic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / Ti(i-PrO)4, (1S,2S)-1,2-N,N'-bis(trifluoromethylsulfonylamino)cyclohexane / toluene

2: 72 percent / pyridine

3: 1.) LiAlD₄, 2.) CrO₃, H₂SO₄ / 1.) Et₂O, 2.) H₂O

With chromium(VI) oxide; titanium(IV) isopropylate; lithium aluminium deuteride; sulfuric acid; C,C,C-trifluoro-N-(2-trifluoromethanesulfonylaminocyclohexyl)methanesulfonamide; In pyridine; toluene;
DOI:10.1021/ja972577v

Reference yield:

: C₁₅H₂₆⁽²⁾H₄O₄

: 199013-53-1,358730-97-9
(12R)-(2,2,3,3,12-2H5)myristic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 83 percent / HCl / methanol

2: 75 percent / (CO)2Cl₂ / dimethylsulfoxide; triethylamine

3: 89 percent / Ti(i-PrO)4, (1S,2S)-1,2-N,N'-bis(trifluoromethylsulfonylamino)cyclohexane / toluene

4: 72 percent / pyridine

5: 1.) LiAlD₄, 2.) CrO₃, H₂SO₄ / 1.) Et₂O, 2.) H₂O

With chromium(VI) oxide; titanium(IV) isopropylate; hydrogenchloride; lithium aluminium deuteride; oxalyl dichloride; sulfuric acid; C,C,C-trifluoro-N-(2-trifluoromethanesulfonylaminocyclohexyl)methanesulfonamide; In pyridine; methanol; dimethyl sulfoxide; triethylamine; toluene;
DOI:10.1021/ja972577v