Docosanoic acid 1-[(R)-2-((2R,3R,4R,5R)-4-acetylamino-5-benzyloxy-3-{(R)-1-[(S)-1-((R)-3-benzyloxycarbonyl-1-carbamoyl-propylcarbamoyl)-ethylcarbamoyl]-ethoxy}-tetrahydro-furan-2-yl)-2-hydroxy-ethoxycarbonyl]-1-methyl-ethyl ester

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Chemical Name:Docosanoic acid 1-[(R)-2-((2R,3R,4R,5R)-4-acetylamino-5-benzyloxy-3-{(R)-1-[(S)-1-((R)-3-benzyloxycarbonyl-1-carbamoyl-propylcarbamoyl)-ethylcarbamoyl]-ethoxy}-tetrahydro-furan-2-yl)-2-hydroxy-ethoxycarbonyl]-1-methyl-ethyl ester
CAS No.:81082-05-5
Molecular Formula:C₅₉H₉₂N₄O₁₄
Molecular Weight:1081.4
Hs Code.:

Docosanoic acid 1-[(R)-2-((2R,3R,4R,5R)-4-acetylamino-5-benzyloxy-3-{(R)-1-[(S)-1-((R)-3-benzyloxycarbonyl-1-carbamoyl-propylcarbamoyl)-ethylcarbamoyl]-ethoxy}-tetrahydro-furan-2-yl)-2-hydroxy-ethoxycarbonyl]-1-methyl-ethyl ester

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Chemical Property of Docosanoic acid 1-[(R)-2-((2R,3R,4R,5R)-4-acetylamino-5-benzyloxy-3-{(R)-1-[(S)-1-((R)-3-benzyloxycarbonyl-1-carbamoyl-propylcarbamoyl)-ethylcarbamoyl]-ethoxy}-tetrahydro-furan-2-yl)-2-hydroxy-ethoxycarbonyl]-1-methyl-ethyl ester

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Technology Process of Docosanoic acid 1-[(R)-2-((2R,3R,4R,5R)-4-acetylamino-5-benzyloxy-3-{(R)-1-[(S)-1-((R)-3-benzyloxycarbonyl-1-carbamoyl-propylcarbamoyl)-ethylcarbamoyl]-ethoxy}-tetrahydro-furan-2-yl)-2-hydroxy-ethoxycarbonyl]-1-methyl-ethyl ester

There total 5 articles about Docosanoic acid 1-[(R)-2-((2R,3R,4R,5R)-4-acetylamino-5-benzyloxy-3-{(R)-1-[(S)-1-((R)-3-benzyloxycarbonyl-1-carbamoyl-propylcarbamoyl)-ethylcarbamoyl]-ethoxy}-tetrahydro-furan-2-yl)-2-hydroxy-ethoxycarbonyl]-1-methyl-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 58886-33-2
benzyl 2-acetamido-2-deoxy-5,6-O-isopropylidene-β-D-glucofuranoside

: 81082-05-5
Docosanoic acid 1-[(R)-2-((2R,3R,4R,5R)-4-acetylamino-5-benzyloxy-3-{(R)-1-[(S)-1-((R)-3-benzyloxycarbonyl-1-carbamoyl-propylcarbamoyl)-ethylcarbamoyl]-ethoxy}-tetrahydro-furan-2-yl)-2-hydroxy-ethoxycarbonyl]-1-methyl-ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) NaH / 1.) 1,4-dioxane, 95 deg C, 1 h, 2.) 1,4-dioxane, 65 deg C, overnight

2: N-methylmorpholine / dimethylformamide / 0.08 h / -15 °C

3: N-methylmorpholine / dimethylformamide / 4 h / -15 °C

4: 96 percent / 65percent aq. AcOH / 5 h / 40 °C

5: 4-(dimethylamino)pyridine, N,N'-dicyclohexylcarbodiimide, / CH₂Cl₂ / 24 h / Ambient temperature

With 4-methyl-morpholine; dmap; sodium hydride; acetic acid; dicyclohexyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00351a005

Reference yield:

: C₂₆H₃₇NO₁₀

: 81082-05-5
Docosanoic acid 1-[(R)-2-((2R,3R,4R,5R)-4-acetylamino-5-benzyloxy-3-{(R)-1-[(S)-1-((R)-3-benzyloxycarbonyl-1-carbamoyl-propylcarbamoyl)-ethylcarbamoyl]-ethoxy}-tetrahydro-furan-2-yl)-2-hydroxy-ethoxycarbonyl]-1-methyl-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: N-methylmorpholine / dimethylformamide / 4 h / -15 °C

2: 96 percent / 65percent aq. AcOH / 5 h / 40 °C

3: 4-(dimethylamino)pyridine, N,N'-dicyclohexylcarbodiimide, / CH₂Cl₂ / 24 h / Ambient temperature

With 4-methyl-morpholine; dmap; acetic acid; dicyclohexyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00351a005

Reference yield:

: 69323-70-2,79982-03-9,81131-16-0
benzyl 2-acetamido-2-deoxy-5,6-O-isopropylidene-3-O-<(R)-2-propionyl-L-alanyl-D-isoglutamine benzyl ester>-β-D-glucofuranoside

: 81082-05-5
Docosanoic acid 1-[(R)-2-((2R,3R,4R,5R)-4-acetylamino-5-benzyloxy-3-{(R)-1-[(S)-1-((R)-3-benzyloxycarbonyl-1-carbamoyl-propylcarbamoyl)-ethylcarbamoyl]-ethoxy}-tetrahydro-furan-2-yl)-2-hydroxy-ethoxycarbonyl]-1-methyl-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / 65percent aq. AcOH / 5 h / 40 °C

2: 4-(dimethylamino)pyridine, N,N'-dicyclohexylcarbodiimide, / CH₂Cl₂ / 24 h / Ambient temperature

With dmap; acetic acid; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1021/jm00351a005