C₄₇H₅₄N₂O₂₀S

Base Information

Chemical Name:C₄₇H₅₄N₂O₂₀S
CAS No.:96201-03-5
Molecular Formula:C₄₇H₅₄N₂O₂₀S
Molecular Weight:999.013
Hs Code.:

C<sub>47</sub>H<sub>54</sub>N<sub>2</sub>O<sub>20</sub>S

Synonyms:

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Chemical Property of C₄₇H₅₄N₂O₂₀S

Chemical Property:

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Technology Process of C₄₇H₅₄N₂O₂₀S

There total 12 articles about C₄₇H₅₄N₂O₂₀S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17236-41-8
((1R,2S,3R,4R,5R)-2,3-Dihydroxy-6,8-dioxa-bicyclo[3.2.1]oct-4-yl)-carbamic acid benzyl ester

: 96201-03-5
C₄₇H₅₄N₂O₂₀S

Guidance literature:: Multi-step reaction with 11 steps

1: 48 percent / Ag₂CO₃, AgClO₄, Drierite / benzene; nitromethane / 2 h / Ambient temperature

2: 65 percent / dibenzo-18-crown-6, sym-collidine, AgClO₄ / benzene; dioxane / 2 h / Ambient temperature

3: NaOMe / methanol / 4 h / Ambient temperature

4: 84 percent / ZnCl₂ / 2 h / Ambient temperature

5: Dowex 1x2(OH^-) / acetone / 1 h / Ambient temperature

6: pyridine

7: HClO₄ / acetone / 1 h / Ambient temperature

8: pyridine / 1.5 h / Ambient temperature

9: pyridine

10: BF₃-Et₂O / tetrahydrofuran / 1.75 h / Ambient temperature

11: pyridine / 5 h / Ambient temperature

With pyridine; 2,4,6-trimethyl-pyridine; calcium sulfate; dibenzo-18-crown-6; perchloric acid; Dowex 1X₂(OH^-); boron trifluoride diethyl etherate; sodium methylate; silver perchlorate; silver carbonate; zinc(II) chloride; In tetrahydrofuran; 1,4-dioxane; methanol; nitromethane; acetone; benzene;
DOI:10.1246/cl.1984.2097

Reference yield:

: 96182-08-0
C₄₀H₃₇NO₁₃

: 96201-03-5
C₄₇H₅₄N₂O₂₀S

Guidance literature:: Multi-step reaction with 10 steps

1: 65 percent / dibenzo-18-crown-6, sym-collidine, AgClO₄ / benzene; dioxane / 2 h / Ambient temperature

2: NaOMe / methanol / 4 h / Ambient temperature

3: 84 percent / ZnCl₂ / 2 h / Ambient temperature

4: Dowex 1x2(OH^-) / acetone / 1 h / Ambient temperature

5: pyridine

6: HClO₄ / acetone / 1 h / Ambient temperature

7: pyridine / 1.5 h / Ambient temperature

8: pyridine

9: BF₃-Et₂O / tetrahydrofuran / 1.75 h / Ambient temperature

10: pyridine / 5 h / Ambient temperature

With pyridine; 2,4,6-trimethyl-pyridine; dibenzo-18-crown-6; perchloric acid; Dowex 1X₂(OH^-); boron trifluoride diethyl etherate; sodium methylate; silver perchlorate; zinc(II) chloride; In tetrahydrofuran; 1,4-dioxane; methanol; acetone; benzene;
DOI:10.1246/cl.1984.2097

Reference yield:

: C₃₉H₄₄N₂O₁₄

: 96201-03-5
C₄₇H₅₄N₂O₂₀S

Guidance literature:: Multi-step reaction with 6 steps

1: pyridine

2: HClO₄ / acetone / 1 h / Ambient temperature

3: pyridine / 1.5 h / Ambient temperature

4: pyridine

5: BF₃-Et₂O / tetrahydrofuran / 1.75 h / Ambient temperature

6: pyridine / 5 h / Ambient temperature

With pyridine; perchloric acid; boron trifluoride diethyl etherate; In tetrahydrofuran; acetone;
DOI:10.1246/cl.1984.2097