Technology Process of 4-Decoxy-benzoyloxy-4'-cyanotolan
There total 9 articles about 4-Decoxy-benzoyloxy-4'-cyanotolan which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 80 percent / pyridine / 24 h / 0 - 20 °C
2: 76 percent / Br2 / CHCl3 / 3 h
3: 26 percent / KOH / ethanol / 24 h / Heating
4: pyridine / 24 h / Ambient temperature
5: 1.) N-methyl-2-pyrrolidone, 2.) ferric chloride, concentrated hydrochloric acid / 1.) 200 deg C, 2 h, 2.) H2O, 60 deg C, 30 min.
With
pyridine; 1-methyl-pyrrolidin-2-one; hydrogenchloride; potassium hydroxide; bromine; iron(III) chloride;
In
ethanol; chloroform;
DOI:10.1080/15421408008084015
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 76 percent / Br2 / CHCl3 / 3 h
2: 26 percent / KOH / ethanol / 24 h / Heating
3: pyridine / 24 h / Ambient temperature
4: 1.) N-methyl-2-pyrrolidone, 2.) ferric chloride, concentrated hydrochloric acid / 1.) 200 deg C, 2 h, 2.) H2O, 60 deg C, 30 min.
With
pyridine; 1-methyl-pyrrolidin-2-one; hydrogenchloride; potassium hydroxide; bromine; iron(III) chloride;
In
ethanol; chloroform;
DOI:10.1080/15421408008084015
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 26 percent / KOH / ethanol / 24 h / Heating
2: pyridine / 24 h / Ambient temperature
3: 1.) N-methyl-2-pyrrolidone, 2.) ferric chloride, concentrated hydrochloric acid / 1.) 200 deg C, 2 h, 2.) H2O, 60 deg C, 30 min.
With
pyridine; 1-methyl-pyrrolidin-2-one; hydrogenchloride; potassium hydroxide; iron(III) chloride;
In
ethanol;
DOI:10.1080/15421408008084015
