2-acetamido>benzoic acid

Base Information

Chemical Name:2-acetamido>benzoic acid
CAS No.:144398-07-2
Molecular Formula:C₂₂H₂₁N₃O₅S
Molecular Weight:439.492
Hs Code.:

2-<N-<3-(4-toluenesulfonamide)phenylamino>acetamido>benzoic acid

Synonyms:

Suppliers and Price of 2-acetamido>benzoic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-acetamido>benzoic acid

Chemical Property:

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Technology Process of 2-acetamido>benzoic acid

There total 1 articles about 2-acetamido>benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 6380-07-0,6272-08-8
N-(3-aminophenyl)-4-methylbenzenesulfonamide

: 14422-49-2
2-chloroacetamidobenzoic acid

: 144398-07-2
2-acetamido>benzoic acid

Guidance literature:: In N,N-dimethyl-formamide; at 80 - 90 ℃; for 4h;
DOI:10.1248/cpb.40.1481

Reference yield:

: 144398-07-2
2-acetamido>benzoic acid

: 144398-08-3
8-(4-toluenesulfonamido)-10H-indolo<3,2-b>quinolin-11-one

Guidance literature:: With PPA; at 120 ℃; for 2h;
DOI:10.1248/cpb.40.1481

Reference yield:

: 144398-07-2
2-acetamido>benzoic acid

: 144398-10-7
N-<4-(8-amino-10H-indolo<3,2-b>quinolin-11-yl)amino-3-methoxyphenyl>methanesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: polyphosphoric acid / 2 h / 120 °C

2: PBr₃ / 10 h / 150 °C

3: 65 percent / 2-ethoxy-ethanol / 5 h / Heating

With PPA; phosphorus tribromide; In 2-ethoxy-ethanol;
DOI:10.1248/cpb.40.1481