2-acetamido-1-N--2-deoxy-β-D-glucopyranosylamine

Base Information

Chemical Name:2-acetamido-1-N--2-deoxy-β-D-glucopyranosylamine
CAS No.:82155-29-1
Molecular Formula:C₃₀H₄₅N₅O₁₂
Molecular Weight:667.714
Hs Code.:

2-acetamido-1-N-<N-(tert-butoxycarbonyl)-L-aspart-1-oyl-(L-phenylalanyl-L-alanine methyl ester)-4-oyl>-2-deoxy-β-D-glucopyranosylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-acetamido-1-N--2-deoxy-β-D-glucopyranosylamine

Chemical Property:

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Technology Process of 2-acetamido-1-N--2-deoxy-β-D-glucopyranosylamine

There total 9 articles about 2-acetamido-1-N--2-deoxy-β-D-glucopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7536-58-5,98482-77-0
BOC-L-aspartic acid 4-benzyl ester

: 82155-29-1
2-acetamido-1-N--2-deoxy-β-D-glucopyranosylamine

Guidance literature:: Multi-step reaction with 4 steps

1: N-methylmorpholine, dicyclohexylcarbodiimide / CHCl₃; dimethylformamide / Ambient temperature

2: 96 percent / hydrogen / Pd black / methanol; acetone

3: dicyclohexylcarbodiimide / dimethylformamide; tetrahydrofuran / 24 h / 0 °C

4: tetrahydrofuran; dimethylformamide / 6 h / Ambient temperature

With 4-methyl-morpholine; hydrogen; dicyclohexyl-carbodiimide; palladium; In tetrahydrofuran; methanol; chloroform; N,N-dimethyl-formamide; acetone;
DOI:10.1016/0008-6215(84)85199-X

Reference yield:

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 82155-29-1
2-acetamido-1-N--2-deoxy-β-D-glucopyranosylamine

Guidance literature:: Multi-step reaction with 6 steps

1: 87 percent / N-methylmorpholine, ethyl chloroformate / dimethylformamide; tetrahydrofuran / Ambient temperature

2: 4.3M HCl / dioxane / 3 h / Ambient temperature

3: N-methylmorpholine, dicyclohexylcarbodiimide / CHCl₃; dimethylformamide / Ambient temperature

4: 96 percent / hydrogen / Pd black / methanol; acetone

5: dicyclohexylcarbodiimide / dimethylformamide; tetrahydrofuran / 24 h / 0 °C

6: tetrahydrofuran; dimethylformamide / 6 h / Ambient temperature

With 4-methyl-morpholine; hydrogenchloride; hydrogen; chloroformic acid ethyl ester; dicyclohexyl-carbodiimide; palladium; In tetrahydrofuran; 1,4-dioxane; methanol; chloroform; N,N-dimethyl-formamide; acetone;
DOI:10.1016/0008-6215(84)85199-X

Reference yield:

: 29847-23-2
2-N-acetylamido-2-deoxy-β-D-glucopyranosyl azide

: 82155-29-1
2-acetamido-1-N--2-deoxy-β-D-glucopyranosylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / hydrogen / PtO₂ (Adam's catalyst) / methanol / 3 h

2: tetrahydrofuran; dimethylformamide / 6 h / Ambient temperature

With hydrogen; platinum(IV) oxide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(84)85199-X