Technology Process of C27H27ClN2O4*ClH
There total 6 articles about C27H27ClN2O4*ClH which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / acetone
2: phosphorus tribromide / chloroform
3: potassium carbonate / toluene
With
phosphorus tribromide; potassium carbonate;
In
chloroform; acetone; toluene;
DOI:10.1016/j.bmc.2012.11.014
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sulfuric acid / 48 h / Reflux
2: potassium carbonate / acetone
3: phosphorus tribromide / chloroform
4: potassium carbonate / toluene
With
sulfuric acid; phosphorus tribromide; potassium carbonate;
In
chloroform; acetone; toluene;
DOI:10.1016/j.bmc.2012.11.014
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium ethanolate / 195 - 200 °C
2: sulfuric acid / 48 h / Reflux
3: potassium carbonate / acetone
4: phosphorus tribromide / chloroform
5: potassium carbonate / toluene
With
sulfuric acid; sodium ethanolate; phosphorus tribromide; potassium carbonate;
In
chloroform; acetone; toluene;
1: |Ullmann Condensation;
DOI:10.1016/j.bmc.2012.11.014