methyl (RS)-5-benzoyloxy-6,7-dihydroxyoctanoate

Base Information

Chemical Name:methyl (RS)-5-benzoyloxy-6,7-dihydroxyoctanoate
CAS No.:86105-87-5
Molecular Formula:C₁₆H₂₂O₆
Molecular Weight:310.347
Hs Code.:

Synonyms:

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Chemical Property of methyl (RS)-5-benzoyloxy-6,7-dihydroxyoctanoate

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Technology Process of methyl (RS)-5-benzoyloxy-6,7-dihydroxyoctanoate

There total 6 articles about methyl (RS)-5-benzoyloxy-6,7-dihydroxyoctanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 86105-86-4
methyl (RS)-5-benzoyloxy-6,7-epoxyoctanoate

: 86105-87-5
methyl (RS)-5-benzoyloxy-6,7-dihydroxyoctanoate

Guidance literature:: With perchloric acid; In 1,4-dioxane; water; for 12h;

Reference yield:

: 100-73-2
acrolein dimer

: 86105-87-5
methyl (RS)-5-benzoyloxy-6,7-dihydroxyoctanoate

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) 50percent NaH / 1.) DMSO, 15 min, 2.) 1 h

2: 60 percent / PCC / CH₂Cl₂

3: Et₃N / 12 h / Ambient temperature

4: 80 percent / 75-80percent MCPBA / CH₂Cl₂ / 18 h

5: 60 percent / Py / 3 h

6: 60 percent / 75percent HClO₄ / various solvent(s); H₂O; dioxane / 12 h

With pyridine; perchloric acid; sodium hydride; triethylamine; 3-chloro-benzenecarboperoxoic acid; pyridinium chlorochromate; In 1,4-dioxane; dichloromethane; water;

Reference yield:

: 80081-22-7
(RS)-2-prop-1-enyl-3,4-dihydro-2H-pyran

: 86105-87-5
methyl (RS)-5-benzoyloxy-6,7-dihydroxyoctanoate

Guidance literature:: Multi-step reaction with 5 steps

1: 60 percent / PCC / CH₂Cl₂

2: Et₃N / 12 h / Ambient temperature

3: 80 percent / 75-80percent MCPBA / CH₂Cl₂ / 18 h

4: 60 percent / Py / 3 h

5: 60 percent / 75percent HClO₄ / various solvent(s); H₂O; dioxane / 12 h

With pyridine; perchloric acid; triethylamine; 3-chloro-benzenecarboperoxoic acid; pyridinium chlorochromate; In 1,4-dioxane; dichloromethane; water;