Technology Process of C61H67N3O3S
There total 4 articles about C61H67N3O3S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C35H37BrN2O3S;
With
tetrakis(triphenylphosphine) palladium(0); sodium carbonate;
In
tetrahydrofuran; water;
at 45 ℃;
for 0.5h;
Inert atmosphere;
(4-(bis(4-(tert-butyl)phenyl)amino)phenyl)boronic acid;
In
tetrahydrofuran; water;
at 80 ℃;
for 16h;
Inert atmosphere;
DOI:10.1039/c3ta10618g
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / tetrahydrofuran; water / 0.5 h / 45 °C / Inert atmosphere
1.2: 16 h / 80 °C / Inert atmosphere
2.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / tetrahydrofuran; water / 0.5 h / 45 °C / Inert atmosphere
2.2: 16 h / 80 °C / Inert atmosphere
With
tetrakis(triphenylphosphine) palladium(0); sodium carbonate;
In
tetrahydrofuran; water;
DOI:10.1039/c3ta10618g
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 20 °C
1.2: 30 h / 20 °C
2.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / tetrahydrofuran; water / 0.5 h / 45 °C / Inert atmosphere
2.2: 16 h / 80 °C / Inert atmosphere
3.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / tetrahydrofuran; water / 0.5 h / 45 °C / Inert atmosphere
3.2: 16 h / 80 °C / Inert atmosphere
With
tetrakis(triphenylphosphine) palladium(0); sodium hydride; sodium carbonate;
In
tetrahydrofuran; water; N,N-dimethyl-formamide; mineral oil;
DOI:10.1039/c3ta10618g
