1-O-<11-<<(2,4,6-Trimethylbenzyl)oxy>carbonyl>undecyl>-2-O-methyl-sn-glyceryl o-chlorophenyl N-(tert-butoxycarbonyl)serine tert-butyl ester phosphate

Base Information

Chemical Name:1-O-<11-<<(2,4,6-Trimethylbenzyl)oxy>carbonyl>undecyl>-2-O-methyl-sn-glyceryl o-chlorophenyl N-(tert-butoxycarbonyl)serine tert-butyl ester phosphate
CAS No.:153959-44-5
Molecular Formula:C₄₄H₆₉ClNO₁₂P
Molecular Weight:870.458
Hs Code.:

1-O-<11-<<(2,4,6-Trimethylbenzyl)oxy>carbonyl>undecyl>-2-O-methyl-sn-glyceryl o-chlorophenyl N-(tert-butoxycarbonyl)serine tert-butyl ester phosphate

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Chemical Property of 1-O-<11-<<(2,4,6-Trimethylbenzyl)oxy>carbonyl>undecyl>-2-O-methyl-sn-glyceryl o-chlorophenyl N-(tert-butoxycarbonyl)serine tert-butyl ester phosphate

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Technology Process of 1-O-<11-<<(2,4,6-Trimethylbenzyl)oxy>carbonyl>undecyl>-2-O-methyl-sn-glyceryl o-chlorophenyl N-(tert-butoxycarbonyl)serine tert-butyl ester phosphate

There total 8 articles about 1-O-<11-<<(2,4,6-Trimethylbenzyl)oxy>carbonyl>undecyl>-2-O-methyl-sn-glyceryl o-chlorophenyl N-(tert-butoxycarbonyl)serine tert-butyl ester phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 505-95-3
12-hydroxydodecanoic acid

: 153959-44-5
1-O-<11-<<(2,4,6-Trimethylbenzyl)oxy>carbonyl>undecyl>-2-O-methyl-sn-glyceryl o-chlorophenyl N-(tert-butoxycarbonyl)serine tert-butyl ester phosphate

Guidance literature:: Multi-step reaction with 5 steps

1: 84 percent / Et₃N / ethyl acetate / 12 h / Heating

2: 60.6 percent / BF₃*Et₂O / CHCl₃ / Ambient temperature

3: NaH / hexane; tetrahydrofuran / 28 h

4: TBAF / tetrahydrofuran / 0.75 h

5: pyridine / tetrahydrofuran / 18 h

With pyridine; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; sodium hydride; triethylamine; In tetrahydrofuran; hexane; chloroform; ethyl acetate;
DOI:10.1021/jo00082a009

Reference yield:

: 71630-31-4,7738-22-9
N-(tert-butyloxycarbonyl)-L-serine tert-butyl ester

: 153959-44-5
1-O-<11-<<(2,4,6-Trimethylbenzyl)oxy>carbonyl>undecyl>-2-O-methyl-sn-glyceryl o-chlorophenyl N-(tert-butoxycarbonyl)serine tert-butyl ester phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / tetrahydrofuran / 4 h

2: pyridine / tetrahydrofuran / 18 h

With pyridine; In tetrahydrofuran;
DOI:10.1021/jo00082a009

Reference yield:

: 1585-16-6
2-chloromethyl-1,3,5-trimethylbenzene

: 153959-44-5
1-O-<11-<<(2,4,6-Trimethylbenzyl)oxy>carbonyl>undecyl>-2-O-methyl-sn-glyceryl o-chlorophenyl N-(tert-butoxycarbonyl)serine tert-butyl ester phosphate

Guidance literature:: Multi-step reaction with 5 steps

1: 84 percent / Et₃N / ethyl acetate / 12 h / Heating

2: 60.6 percent / BF₃*Et₂O / CHCl₃ / Ambient temperature

3: NaH / hexane; tetrahydrofuran / 28 h

4: TBAF / tetrahydrofuran / 0.75 h

5: pyridine / tetrahydrofuran / 18 h

With pyridine; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; sodium hydride; triethylamine; In tetrahydrofuran; hexane; chloroform; ethyl acetate;
DOI:10.1021/jo00082a009