Fumaric acid didecyl ester

Base Information

Chemical Name:Fumaric acid didecyl ester
CAS No.:16669-28-6
Molecular Formula:C₂₄H₄₄O₄
Molecular Weight:396.611
Hs Code.:
DSSTox Substance ID:DTXSID80874009
Nikkaji Number:J114.837K
Wikidata:Q81981383

Synonyms:Di-n-decyl fumarate;Fumaric acid didecyl ester;SCHEMBL781039;SCHEMBL2339552;DTXSID80874009;16669-28-6

Suppliers and Price of Fumaric acid didecyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Fumaric acid didecyl ester

Chemical Property:

XLogP3:9.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:22
Exact Mass:396.32395988
Heavy Atom Count:28
Complexity:354

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCCCCCCCCCOC(=O)C=CC(=O)OCCCCCCCCCC
Isomeric SMILES:CCCCCCCCCCOC(=O)/C=C/C(=O)OCCCCCCCCCC

Technology Process of Fumaric acid didecyl ester

There total 3 articles about Fumaric acid didecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 112-30-1
1-Decanol

: 364745-47-1
(3-decyloxycarbonyl)acrylic acid

: 6290-56-8,45298-06-4,16669-28-6
di-n-decyl fumarate

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 24h; under 760.051 Torr; Inert atmosphere;
DOI:10.1021/acs.joc.6b00526

Reference yield:

: 627-63-4
fumaryl dichloride

: 112-30-1
1-Decanol

: 6290-56-8,45298-06-4,16669-28-6
di-n-decyl fumarate

Guidance literature:: With N,N-dimethyl-aniline; In tetrahydrofuran; at 49.85 ℃;
DOI:10.1039/a904815d

Reference yield:

: 112-30-1
1-Decanol

: 6290-56-8,45298-06-4,16669-28-6
di-n-decyl fumarate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 1 h / 55 °C / 760.05 Torr / Inert atmosphere

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 24 h / 20 °C / 760.05 Torr / Inert atmosphere

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane;
DOI:10.1021/acs.joc.6b00526