N^α-(2-naphthylsulfonyl)-3-cyano-DL-phenylalanyl chloride

Base Information

Chemical Name:N^α-(2-naphthylsulfonyl)-3-cyano-DL-phenylalanyl chloride
CAS No.:80852-52-4
Molecular Formula:C₂₀H₁₅ClN₂O₃S
Molecular Weight:398.87
Hs Code.:

N<sup>α</sup>-(2-naphthylsulfonyl)-3-cyano-DL-phenylalanyl chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N^α-(2-naphthylsulfonyl)-3-cyano-DL-phenylalanyl chloride

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Technology Process of N^α-(2-naphthylsulfonyl)-3-cyano-DL-phenylalanyl chloride

There total 7 articles about N^α-(2-naphthylsulfonyl)-3-cyano-DL-phenylalanyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 93-11-8
2-Naphthalenesulfonyl chloride

: 80852-52-4
N^α-(2-naphthylsulfonyl)-3-cyano-DL-phenylalanyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: N-methylmorpholine / dioxane; ethyl acetate / 16 h / Ambient temperature

2: 1N aq. HCl, AcOH / 2 h / Heating

3: SOCl₂ / 1 h / Heating

With 4-methyl-morpholine; hydrogenchloride; thionyl chloride; acetic acid; In 1,4-dioxane; ethyl acetate;
DOI:10.1021/jm960668h

Reference yield:

: 3-cyano-DL-phenylalanine methyl ester hydrochloride

: 80852-52-4
N^α-(2-naphthylsulfonyl)-3-cyano-DL-phenylalanyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: N-methylmorpholine / dioxane; ethyl acetate / 16 h / Ambient temperature

2: 1N aq. HCl, AcOH / 2 h / Heating

3: SOCl₂ / 1 h / Heating

With 4-methyl-morpholine; hydrogenchloride; thionyl chloride; acetic acid; In 1,4-dioxane; ethyl acetate;
DOI:10.1021/jm960668h