C₅H₄CH₃Fe(CO)(P(C₆H₅)3)C⁽²⁾H₃

Base Information

• Chemical Name: C₅H₄CH₃Fe(CO)(P(C₆H₅)3)C⁽²⁾H₃
• CAS No.: 97011-44-4
• Molecular Formula: C₂₆H₂₅FeOP
• Molecular Weight: 443.281
• Mol file: 97011-44-4.mol

Synonyms:

Chemical Property of C₅H₄CH₃Fe(CO)(P(C₆H₅)3)C⁽²⁾H₃

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of C₅H₄CH₃Fe(CO)(P(C₆H₅)3)C⁽²⁾H₃

There total 1 articles about C₅H₄CH₃Fe(CO)(P(C₆H₅)3)C⁽²⁾H₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

{(η5-C5H5)(CO)Fe(μ-CO)(μ-COCH3)Mn(CO)(η5-MeC5H4)} + CH3C5H4Fe(CO)3Mn(C5H4CH3)(COC(2)H3) + triphenylphosphine (603-35-0) → C5H4CH3Fe(CO)(P(C6H5)3)C(2)H3 (97011-44-4) + (C5H4CH3)Fe(CO)(P(C6H5)3)(CH3) + (cyclopentadienyl)(CO)(PPh3)Fe(CH3) + C5H5Fe(CO)(P(C6H5)3)C(2)H3 (863608-79-1)

Guidance literature:

In benzene-d6; heating a soln. of complexes and phosphine in C6D6 at 65 or 75°C; not isolated, detected by NMR; Kinetics;

DOI:10.1021/om0502640

Reference yield:

C5H4CH3Fe(CO)(P(C6H5)3)C(2)H3 (97011-44-4) + {(η5-C5H5)(CO)Fe(μ-CO)(μ-COCH3)Mn(CO)(η5-MeC5H4)} → methylcyclopentadienyl manganese(I) tricarbonyl + (C5H4CH3)Fe(CO)(P(C6H5)3)(CH3) + (cyclopentadienyl)(CO)(PPh3)Fe(CH3)

Guidance literature:

With triphenylphosphine; In benzene; heating a benzene soln. with 1.2 equiv of PPh3 at 65°C; not sepd., detected by NMR;

Reference yield:

C5H4CH3Fe(CO)(P(C6H5)3)C(2)H3 (97011-44-4) + (cyclopentadienyl)(CO)(PPh3)Fe(CH3) + triphenylphosphine (603-35-0) → (C5H4CH3)Fe(CO)(P(C6H5)3)(CH3)

Guidance literature:

In benzene-d6; heating a soln. of complexes and phosphine in C6D6 at 75°C; not isolated, detected by NMR;

DOI:10.1021/om0502640

upstream raw materials:

triphenylphosphine