{rhodium(1,2-bis(diphenylphosphino)butane)(NBD)}perchlorate*CH₂Cl₂

Base Information

Chemical Name:{rhodium(1,2-bis(diphenylphosphino)butane)(NBD)}perchlorate*CH₂Cl₂
CAS No.:112712-01-3
Molecular Formula:CH₂Cl₂*C₃₅H₃₆P₂Rh*ClO₄
Molecular Weight:805.907
Hs Code.:

{rhodium(1,2-bis(diphenylphosphino)butane)(NBD)}perchlorate*CH<sub>2</sub>Cl<sub>2</sub>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {rhodium(1,2-bis(diphenylphosphino)butane)(NBD)}perchlorate*CH₂Cl₂

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Technology Process of {rhodium(1,2-bis(diphenylphosphino)butane)(NBD)}perchlorate*CH₂Cl₂

There total 1 articles about {rhodium(1,2-bis(diphenylphosphino)butane)(NBD)}perchlorate*CH₂Cl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 60576-58-1
{Rh(NBD)2}ClO₄

: 7688-25-7
1,4-di(diphenylphosphino)-butane

: 112712-01-3
{rhodium(1,2-bis(diphenylphosphino)butane)(NBD)}perchlorate*CH₂Cl₂

Guidance literature:: In dichloromethane; addn. of the phosphine in small portions over 30 sec to a stirred soln. of the Rh compd. in deoxygenated CH2Cl2 under Ar, stirring for 5 min; filtn. under Ar through Celite, washing with CH2Cl2, evapn., dropwise addn. of abs. deoxygenated diethyl ether, standing, filtn., washing with ether-CH2Cl2 and ether and drying under a Ar flow;
DOI:10.1021/om00094a025