N-Hydroxy-4-[(methylamino)sulfonyl]benzeneethanimidamide

Base Information

Chemical Name:N-Hydroxy-4-[(methylamino)sulfonyl]benzeneethanimidamide
CAS No.:148459-02-3
Molecular Formula:C₉H₁₃N₃O₃S
Molecular Weight:243.287
Hs Code.:
DSSTox Substance ID:DTXSID901200426

Synonyms:DTXSID901200426;N-Hydroxy-4-[(methylamino)sulfonyl]benzeneethanimidamide;148459-02-3

Suppliers and Price of N-Hydroxy-4-[(methylamino)sulfonyl]benzeneethanimidamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of N-Hydroxy-4-[(methylamino)sulfonyl]benzeneethanimidamide

Chemical Property:

XLogP3:0
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:4
Exact Mass:243.06776246
Heavy Atom Count:16
Complexity:340

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CNS(=O)(=O)C1=CC=C(C=C1)CC(=NO)N
Isomeric SMILES:CNS(=O)(=O)C1=CC=C(C=C1)C/C(=N/O)/N

Technology Process of N-Hydroxy-4-[(methylamino)sulfonyl]benzeneethanimidamide

There total 3 articles about N-Hydroxy-4-[(methylamino)sulfonyl]benzeneethanimidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 148459-08-9
4-((N-methylamino)sulfonyl)benzyl cyanide

: 148459-02-3
N-Hydroxy-2-(4-methylsulfamoyl-phenyl)-acetamidine

Guidance literature:: With hydroxylamine hydrochloride; sodium; In methanol; a) reflux, 2 h, b) 25 deg C, 16 h;
DOI:10.1021/jm00063a003

Reference yield:

: 148459-00-1
4-(bromomethyl)-N-methylbenzenesulfonamide

: 148459-02-3
N-Hydroxy-2-(4-methylsulfamoyl-phenyl)-acetamidine

Guidance literature:: Multi-step reaction with 2 steps

1: 8.58 g / ethanol; H₂O / 4 h / Heating

2: NH₂OH*HCl, Na / methanol / a) reflux, 2 h, b) 25 deg C, 16 h

With hydroxylamine hydrochloride; sodium; In methanol; ethanol; water;
DOI:10.1021/jm00063a003

Reference yield:

: 640-61-9
N-methyl-p-toluenesulfonylamide

: 148459-02-3
N-Hydroxy-2-(4-methylsulfamoyl-phenyl)-acetamidine

Guidance literature:: Multi-step reaction with 3 steps

1: 32.1 g / N-bromosuccinimide, benzoyl peroxide / CCl₄ / 3 h / Heating; Irradiation

2: 8.58 g / ethanol; H₂O / 4 h / Heating

3: NH₂OH*HCl, Na / methanol / a) reflux, 2 h, b) 25 deg C, 16 h

With N-Bromosuccinimide; Perbenzoic acid; hydroxylamine hydrochloride; sodium; In methanol; tetrachloromethane; ethanol; water;
DOI:10.1021/jm00063a003