Technology Process of 6-bromo-3,4-diethoxybenzaldehyde dimethyl acetal
There total 1 articles about 6-bromo-3,4-diethoxybenzaldehyde dimethyl acetal which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: n-BuLi / tetrahydrofuran / 0.25 h / -78 °C
1.2: tetrahydrofuran / 0.5 h / -40 °C
2.1: 2 N HCl / tetrahydrofuran / 20 °C
With
hydrogenchloride; n-butyllithium;
In
tetrahydrofuran;
DOI:10.1021/jm000558h
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: n-BuLi / tetrahydrofuran / 0.25 h / -78 °C
1.2: tetrahydrofuran / 0.5 h / -40 °C
2.1: 2 N HCl / tetrahydrofuran / 20 °C
3.1: resorcinol; acetate buffer; NaClO2 / dioxane; H2O / 20 °C / pH 3.8
With
hydrogenchloride; sodium chlorite; n-butyllithium; acetate buffer; recorcinol;
In
tetrahydrofuran; 1,4-dioxane; water;
DOI:10.1021/jm000558h
