Technology Process of C16H11ClN2S
There total 4 articles about C16H11ClN2S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: acetic acid / water
2: trichlorophosphate / 0 - 90 °C
3: sodium sulfide / N,N-dimethyl-formamide / 20 °C
4: sulfuric acid / ethanol / Reflux
With
sodium sulfide; sulfuric acid; acetic acid; trichlorophosphate;
In
ethanol; water; N,N-dimethyl-formamide;
2: |Vilsmeier Reaction;
DOI:10.1007/s00044-012-0060-8
- Guidance literature:
-
Multi-step reaction with 3 steps
1: trichlorophosphate / 0 - 90 °C
2: sodium sulfide / N,N-dimethyl-formamide / 20 °C
3: sulfuric acid / ethanol / Reflux
With
sodium sulfide; sulfuric acid; trichlorophosphate;
In
ethanol; N,N-dimethyl-formamide;
1: |Vilsmeier Reaction;
DOI:10.1007/s00044-012-0060-8
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium sulfide / N,N-dimethyl-formamide / 20 °C
2: sulfuric acid / ethanol / Reflux
With
sodium sulfide; sulfuric acid;
In
ethanol; N,N-dimethyl-formamide;
DOI:10.1007/s00044-012-0060-8