1,3,5-tris(aminomethyl)-2,4,6-tributylbenzene

Base Information

Chemical Name:1,3,5-tris(aminomethyl)-2,4,6-tributylbenzene
CAS No.:400886-01-3
Molecular Formula:C₂₁H₃₉N₃
Molecular Weight:333.561
Hs Code.:

Synonyms:

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Chemical Property of 1,3,5-tris(aminomethyl)-2,4,6-tributylbenzene

Chemical Property:

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Technology Process of 1,3,5-tris(aminomethyl)-2,4,6-tributylbenzene

There total 4 articles about 1,3,5-tris(aminomethyl)-2,4,6-tributylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 400886-02-4
1,3,5-tributyl-2,4,6-tris(phthalimidomethyl)benzene

: 400886-01-3
1,3,5-tris(aminomethyl)-2,4,6-tributylbenzene

Guidance literature:: 1,3,5-tributyl-2,4,6-tris(phthalimidomethyl)benzene; With hydrazine hydrate; In ethanol; for 0.5h; Heating;

With hydrogenchloride; In water; for 0.5h; Further stages.; Heating;
DOI:10.1039/b105913k

Reference yield:

: 108-70-3,63697-19-8
1,3,5-trichlorobenzene

: 400886-01-3
1,3,5-tris(aminomethyl)-2,4,6-tributylbenzene

Guidance literature:: Multi-step reaction with 4 steps

1.1: 31.4 g / NiCl₂(DPPP) / diethyl ether

2.1: 17.5 g / conc. H₂SO₄ / 18 h / Heating

3.1: 1.39 g / dimethylformamide / 3 h / 60 °C

4.1: NH₂NH₂*H₂O / ethanol / 0.5 h / Heating

4.2: 64 percent / 6 M HCl / H₂O / 0.5 h / Heating

With sulfuric acid; hydrazine hydrate; 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); In diethyl ether; ethanol; N,N-dimethyl-formamide; 1.1: Grignard reaction / 4.1: Gabriel reaction;
DOI:10.1039/b105913k

Reference yield:

: 841-07-6
1,3,5-tributylbenzene

: 400886-01-3
1,3,5-tris(aminomethyl)-2,4,6-tributylbenzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: 17.5 g / conc. H₂SO₄ / 18 h / Heating

2.1: 1.39 g / dimethylformamide / 3 h / 60 °C

3.1: NH₂NH₂*H₂O / ethanol / 0.5 h / Heating

3.2: 64 percent / 6 M HCl / H₂O / 0.5 h / Heating

With sulfuric acid; hydrazine hydrate; In ethanol; N,N-dimethyl-formamide; 3.1: Gabriel reaction;
DOI:10.1039/b105913k