7,9-Ph₂-nido-7,9-P₂B₉H₉

Base Information

• Chemical Name: 7,9-Ph₂-nido-7,9-P₂B₉H₉
• CAS No.: 620170-81-2
• Molecular Formula: C₁₂H₁₉B₉P₂
• Molecular Weight: 322.529

Synonyms:

Chemical Property of 7,9-Ph₂-nido-7,9-P₂B₉H₉

Chemical Property:

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Technology Process of 7,9-Ph₂-nido-7,9-P₂B₉H₉

There total 1 articles about 7,9-Ph₂-nido-7,9-P₂B₉H₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

(CH3)4N[nido-B9H12] + Dichlorophenylphosphine (644-97-3) → Ph-nido-PB9H11 + 7,9-Ph2-nido-7,9-P2B9H9 (620170-81-2)

Guidance literature:

With NaH; In 1,2-dimethoxyethane; byproducts: NaCl, H2, (CH3)4NCl; mixt. of B compound, NaH, and PhPCl2 in 1,2-dimethoxyethane heated at 80°C for 39 h under an inert atmosphere; preparative TLC (hexanes/CH2Cl2 (4/1)); elem. anal.;

DOI:10.1016/S0022-328X(03)00165-7

upstream raw materials:

Dichlorophenylphosphine

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